(1H-Indol-6-yl)acetylene

Base Information

Chemical Name:(1H-Indol-6-yl)acetylene
CAS No.:865375-93-5
Molecular Formula:C₁₀H₇N
Molecular Weight:141.172
Hs Code.:2933998090
Mol file:865375-93-5.mol

Synonyms:(1H-Indol-6-yl)acetylene;6-Ethynyl-1H-indole

Suppliers and Price of (1H-Indol-6-yl)acetylene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
6-Ethynyl-1H-indole
1g
$ 763.68

Total 5 raw suppliers

Chemical Property of (1H-Indol-6-yl)acetylene

Chemical Property:

PSA：15.79000
LogP:2.14920

Purity/Quality:

98% ^*data from raw suppliers

6-Ethynyl-1H-indole ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (1H-Indol-6-yl)acetylene

There total 6 articles about (1H-Indol-6-yl)acetylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 899792-76-8
2-acetylamino-1,4-diethynylbenzene

: 865375-93-5
6-ethynylindole

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 13h;
DOI:10.1007/s11172-006-0160-z

Reference yield:

: 2-nitro-1,4-bis(1,3,3-trimethylindolin-2-ylideneacetyl)benzene

: 865375-93-5
6-ethynylindole

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / POCl₃ / dioxane / 6 h / 90 °C

2: Zn; aq. NH₄OH / 48 h / 20 °C

3: 1.42 g / benzene / 4 h / Heating

4: 45 percent / NaH / dimethylformamide / 13 h

With ammonium hydroxide; sodium hydride; zinc; trichlorophosphate; In 1,4-dioxane; N,N-dimethyl-formamide; benzene;
DOI:10.1007/s11172-006-0160-z

Reference yield:

: 610-29-7
2-nitroterephthalic acid

: 865375-93-5
6-ethynylindole

Guidance literature:: Multi-step reaction with 6 steps

1: thionyl chloride / dimethylformamide; benzene / Heating

2: 84 g / Et₃N / benzene / 24 h / 20 °C

3: 78 percent / POCl₃ / dioxane / 6 h / 90 °C

4: Zn; aq. NH₄OH / 48 h / 20 °C

5: 1.42 g / benzene / 4 h / Heating

6: 45 percent / NaH / dimethylformamide / 13 h

With ammonium hydroxide; thionyl chloride; sodium hydride; triethylamine; zinc; trichlorophosphate; In 1,4-dioxane; N,N-dimethyl-formamide; benzene;
DOI:10.1007/s11172-006-0160-z