Methyl 3-cyclopropoxybenzoate

Base Information

• Chemical Name: Methyl 3-cyclopropoxybenzoate
• CAS No.: 921602-60-0
• Molecular Formula: C₁₁H₁₂O₃
• Molecular Weight: 192.214
• Hs Code.: 2918990090
• Mol file: 921602-60-0.mol

Synonyms:Methyl 3-cyclopropoxybenzoate;3-Cyclopropoxy-benzoic acid Methyl ester

Chemical Property of Methyl 3-cyclopropoxybenzoate

Chemical Property:

• PSA: 35.53000
• LogP: 2.01440
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

Methyl3-cyclopropoxybenzoate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 3-cyclopropoxybenzoate

There total 3 articles about Methyl 3-cyclopropoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diiodomethane (75-11-6) + methyl 3-(vinyloxy)benzoate (61031-63-8) → methyl 3-cyclopropoxybenzoate (921602-60-0)

Guidance literature:

With diethylzinc; In dichloromethane; at 0 - 20 ℃; for 5h;

Reference yield:

1-Bromo-2-(3'-carbomethoxyphenoxy)ethane (59516-96-0) → methyl 3-cyclopropoxybenzoate (921602-60-0)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium tert-butylate / tetrahydrofuran / 5 h

2: diethylzinc / dichloromethane / 5 h / 0 - 20 °C

With potassium tert-butylate; diethylzinc; In tetrahydrofuran; dichloromethane;

Reference yield:

methyl 3-hydroxybenzoate (19438-10-9) → methyl 3-cyclopropoxybenzoate (921602-60-0)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 24 h

2: potassium tert-butylate / tetrahydrofuran / 5 h

3: diethylzinc / dichloromethane / 5 h / 0 - 20 °C

With potassium tert-butylate; diethylzinc; potassium carbonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

upstream raw materials:

1-Bromo-2-(3'-carbomethoxyphenoxy)ethane

diiodomethane

methyl 3-(vinyloxy)benzoate

methyl 3-hydroxybenzoate

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