4-CHLORO-3-IODOBENZALDOXIME

Base Information

Chemical Name:4-CHLORO-3-IODOBENZALDOXIME
CAS No.:914106-25-5
Molecular Formula:C7H5ClINO
Molecular Weight:281.48
Hs Code.:
Mol file:914106-25-5.mol

Synonyms:4-CHLORO-3-IODOBENZALDOXIME

Suppliers and Price of 4-CHLORO-3-IODOBENZALDOXIME

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(E)-N-[(4-CHLORO-3-IODOPHENYL)METHYLIDENE]HYDROXYLAMINE 95.00%
5MG
$ 504.56

Total 1 raw suppliers

Chemical Property of 4-CHLORO-3-IODOBENZALDOXIME

Chemical Property:

PSA：32.59000
LogP:2.75270

Purity/Quality:

99% ^*data from raw suppliers

(E)-N-[(4-CHLORO-3-IODOPHENYL)METHYLIDENE]HYDROXYLAMINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-CHLORO-3-IODOBENZALDOXIME

There total 1 articles about 4-CHLORO-3-IODOBENZALDOXIME which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 276866-90-1
4-chloro-3-iodobenzaldehyde

: 914106-25-5
4-chloro-3-iodobenzaldoxime

Guidance literature:: With pyridine; hydroxylamine hydrochloride; In ethanol;
DOI:10.1021/jm0612867

Reference yield: 91.0%

: 914106-25-5
4-chloro-3-iodobenzaldoxime

: 914106-26-6
4-chloro-3-iodobenzonitrile

Guidance literature:: With acetic anhydride; for 4h; Heating;
DOI:10.1021/jm0612867

Reference yield:

: 914106-25-5
4-chloro-3-iodobenzaldoxime

: 914106-16-4
3-(4-cyanophenyl)-5-(2-chloro-5-cyanophenyl)isoxazole

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / Ac₂O / 4 h / Heating

2: 88 percent / Et₃N / PdCl₂(PPh₃)2; CuI / 3 h / 60 °C

3: 62 percent / aq. cesium carbonate / acetonitrile / 120 h / 0 °C

4: 32 percent / bis(tributyltin) oxide / CH₂Cl₂

With acetic anhydride; caesium carbonate; triethylamine; bis(tri-n-butyltin)oxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In dichloromethane; acetonitrile;
DOI:10.1021/jm0612867