2-{[(4-BROMOPHENYL)SULPHONYL]AMINO)}BENZAMIDE

Base Information

• Chemical Name: 2-{[(4-BROMOPHENYL)SULPHONYL]AMINO)}BENZAMIDE
• CAS No.: 333441-46-6
• Molecular Formula: C₁₃H₁₁BrN₂O₃S
• Molecular Weight: 355.212
• Hs Code.: 2935909099

Synonyms:2-{[(4-BROMOPHENYL)SULPHONYL]AMINO)}BENZAMIDE;2-[(4-Bromophenyl)sulphonamido]benzamide, 4-Bromo-N-(2-carbamoylphenyl)benzenesulphonamide;2-{[(4-Bromophenyl)sulfonyl]-amino}benzenecarboxamide

Chemical Property of 2-{[(4-BROMOPHENYL)SULPHONYL]AMINO)}BENZAMIDE

Chemical Property:

• PSA: 98.63000
• LogP: 4.38680

Purity/Quality:

99% ^*data from raw suppliers

2-{[(4-Bromophenyl)sulfonyl]-amino}benzenecarboxamide >90% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-{[(4-BROMOPHENYL)SULPHONYL]AMINO)}BENZAMIDE

There total 3 articles about 2-{[(4-BROMOPHENYL)SULPHONYL]AMINO)}BENZAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

2-((4-bromophenyl)sulfonamido)benzoic acid (51012-29-4) → 2-(4-bromophenylsulfonamido)benzamide (333441-46-6)

Guidance literature:

2-((4-bromophenyl)sulfonamido)benzoic acid; With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; for 0.166667h;

With ammonia; In methanol; N,N-dimethyl-formamide;

DOI:10.1039/c9md00088g

Reference yield:

anthranilic acid (118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4) → 2-(4-bromophenylsulfonamido)benzamide (333441-46-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium carbonate / water / 60 °C

2: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 0.17 h

With sodium carbonate; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In water; N,N-dimethyl-formamide;

DOI:10.1039/c9md00088g

Reference yield:

4-bromobenzenesulfonyl chloride (98-58-8) → 2-(4-bromophenylsulfonamido)benzamide (333441-46-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium carbonate / water / 60 °C

2: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 0.17 h

With sodium carbonate; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In water; N,N-dimethyl-formamide;

DOI:10.1039/c9md00088g

upstream raw materials:

anthranilic acid

4-bromobenzenesulfonyl chloride

2-((4-bromophenyl)sulfonamido)benzoic acid

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