(4-Boc-1-piperaziniuM-1-ylMethyl)trifluoroborate internal salt, 95%

Base Information

• Chemical Name: (4-Boc-1-piperaziniuM-1-ylMethyl)trifluoroborate internal salt, 95%
• CAS No.: 1268340-97-1
• Molecular Formula: C10H20BF3N2O2
• Molecular Weight: 268.0842096
• Hs Code.: 2933998087
• Mol file: 1268340-97-1.mol

Synonyms:(4-Boc-1-piperaziniuM-1-ylMethyl)trifluoroborate internal salt, 95%

Chemical Property of (4-Boc-1-piperaziniuM-1-ylMethyl)trifluoroborate internal salt, 95%

Chemical Property:

• Melting Point: 185℃
• PSA: 32.78000
• LogP: 2.21980

Purity/Quality:

99%, ^*data from raw suppliers

(4-Boc-1-piperazinium-1-ylmethyl)trifluoroborateinternalsalt 98+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (4-Boc-1-piperaziniuM-1-ylMethyl)trifluoroborate internal salt, 95%

There total 1 articles about (4-Boc-1-piperaziniuM-1-ylMethyl)trifluoroborate internal salt, 95% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

potassium chloromethyltrifluoroborate + 1-t-Butoxycarbonylpiperazine (57260-71-6) → 4-trifluoroboratomethylpiperazine-1-carboxylic acid tert-butyl ester internal salt (1268340-97-1)

Guidance literature:

In tetrahydrofuran; tert-butyl alcohol; at 80 ℃; for 6.5h; Inert atmosphere;

DOI:10.1021/jo2001066

Reference yield: 98.0%

4-chloromethoxybenzene (623-12-1) + 4-trifluoroboratomethylpiperazine-1-carboxylic acid tert-butyl ester internal salt (1268340-97-1) → 4-(4-methoxybenzyl)piperazine-1-carboxylic acid tert-butyl ester (936330-00-6)

Guidance literature:

With palladium diacetate; caesium carbonate; XPhos; In tetrahydrofuran; water; at 80 ℃; for 45h;

DOI:10.1021/jo2001066

Reference yield:

4-trifluoroboratomethylpiperazine-1-carboxylic acid tert-butyl ester internal salt (1268340-97-1) → potassium 4-(trifluoroboratomethyl)piperazine-1-carboxylic acid tert-butyl ester

Guidance literature:

With potassium phosphate; In acetone;

DOI:10.1021/jo2001066

upstream raw materials:

1-t-Butoxycarbonylpiperazine

Downstream raw materials:

4-(4-methoxybenzyl)piperazine-1-carboxylic acid tert-butyl ester

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