1,6-diMethyl-2,3-dihydroquinolin-4-one

Base Information

• Chemical Name: 1,6-diMethyl-2,3-dihydroquinolin-4-one
• CAS No.: 959699-02-6
• Molecular Formula: C11H13NO
• Molecular Weight: 175.23
• Hs Code.: 2933499090
• Mol file: 959699-02-6.mol

Synonyms:1,6-diMethyl-2,3-dihydroquinolin-4-one;1,6-DiMethyl-2,3-dihydroquinolin-4(1H)-one

Chemical Property of 1,6-diMethyl-2,3-dihydroquinolin-4-one

Chemical Property:

• PSA: 20.31000
• LogP: 2.08260
• Storage Temp.: 2-8°C

Purity/Quality:

95+% ^*data from raw suppliers

1,6-Dimethyl-2,3-dihydroquinolin-4(1H)-one 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,6-diMethyl-2,3-dihydroquinolin-4-one

There total 4 articles about 1,6-diMethyl-2,3-dihydroquinolin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

methyl 3-[N-(2-iodo-4-methylphenyl)-N-methylamino]propionate (959698-50-1) → 1,6-dimethyl-2,3-dihydro-1H-quinolin-4-one (959699-02-6) + methyl 3-[N-methyl-N-(4-methylphenyl)amino]propionate (2003-73-8)

Guidance literature:

With potassium phosphate; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 110 ℃; for 72h;

DOI:10.1002/anie.200702176

Reference yield: 65.0%

3-[N-(2-iodo-4-methylphenyl)-N-methylamino]-N-methoxy-N-methylpropanamide (1088708-51-3) → 1,6-dimethyl-2,3-dihydro-1H-quinolin-4-one (959699-02-6) + C13H20N2O2

Guidance literature:

With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In toluene; at 110 ℃; for 48h; Sealed tube;

DOI:10.1021/jo8020715

Reference yield: 64.0%

methyl 3-[N-(2-bromo-4-methylphenyl)-N-methylamino]propionate (959698-53-4) → 1,6-dimethyl-2,3-dihydro-1H-quinolin-4-one (959699-02-6) + methyl 3-[N-methyl-N-(4-methylphenyl)amino]propionate (2003-73-8)

Guidance literature:

With potassium phosphate; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 110 ℃; for 72h;

DOI:10.1002/anie.200702176

upstream raw materials:

methyl 3-[N-(2-iodo-4-methylphenyl)-N-methylamino]propionate

benzyl 3-[N-(2-iodo-4-methylphenyl)-N-methylamino]propionate

methyl 3-[N-(2-bromo-4-methylphenyl)-N-methylamino]propionate

3-[N-(2-iodo-4-methylphenyl)-N-methylamino]-N-methoxy-N-methylpropanamide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 959699-02-6 1,6-diMethyl-2,3-dihydroquinolin-4-one

Send

Send

Metric Ton KG G Pound L ML

Send

Send