Ethyl 5-hydroxypyridine-2...

Base Information

• Chemical Name: Ethyl 5-hydroxypyridine-2...
• CAS No.: 132807-30-8
• Molecular Formula: C9H11NO3
• Molecular Weight: 181.18854
• Hs Code.: 2933399090
• Mol file: 132807-30-8.mol

Synonyms:Ethyl 5-hydroxypyridine-2...;Ethyl 5-hydroxypyridine-2-acetate;ethyl 2-(5-hydroxypyridin-2-yl)acetate;Ethyl 2-(5-hydroxypyridin-2-yl)

Chemical Property of Ethyl 5-hydroxypyridine-2...

Chemical Property:

• PSA: 59.42000
• LogP: 0.89280

Purity/Quality:

99%, ^*data from raw suppliers

ethyl2-(5-hydroxypyridin-2-yl)acetate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Ethyl 5-hydroxypyridine-2...

There total 3 articles about Ethyl 5-hydroxypyridine-2... which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

ethyl 5-benzyloxy-2-pyridylacetate (132807-20-6) → ethyl 2-(5-hydroxypyridin-2-yl)acetate (132807-30-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; under 49400 Torr; Ambient temperature;

Reference yield:

5-benzyloxy-2-cyanomethylpyridine (132807-32-0) → ethyl 2-(5-hydroxypyridin-2-yl)acetate (132807-30-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 66 percent / HCl

2: 90 percent / H₂ / 10percent Pd/C / ethanol / 49400 Torr / Ambient temperature

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol;

Reference yield:

5-benzyloxy-2-chloromethylpyridine hydrochloride (132807-31-9) → ethyl 2-(5-hydroxypyridin-2-yl)acetate (132807-30-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 84 percent

2: 66 percent / HCl

3: 90 percent / H₂ / 10percent Pd/C / ethanol / 49400 Torr / Ambient temperature

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol;

upstream raw materials:

ethyl 5-benzyloxy-2-pyridylacetate

5-benzyloxy-2-cyanomethylpyridine

5-benzyloxy-2-chloromethylpyridine hydrochloride

Downstream raw materials:

ethyl 5-benzoyloxy-2-pyridylacetate

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