N-(4-amino-2-methylphenyl)furan-2-carboxamide

Base Information

• Chemical Name: N-(4-amino-2-methylphenyl)furan-2-carboxamide
• CAS No.: 404832-64-0
• Molecular Formula: C₁₂H₁₂N₂O₂
• Molecular Weight: 216.239
• Hs Code.: 2932190090
• European Community (EC) Number: 875-179-9
• DSSTox Substance ID: DTXSID70352982
• Wikidata: Q82130428
• Mol file: 404832-64-0.mol

Synonyms:404832-64-0;N-(4-amino-2-methylphenyl)furan-2-carboxamide;N-(4-Amino-2-methylphenyl)-2-furamide;Furan-2-carboxylic acid (4-amino-2-methyl-phenyl)-amide;Cambridge id 6023960;Oprea1_379795;Oprea1_674335;DTXSID70352982;BBL000078;MFCD02018047;STK085497;AKOS000108397;SB61211;SDCCGMLS-0064960.P001;VS-00431;BB 0245293;CS-0216587;EN300-51893;N-(4-amino-2-methylphenyl)-2-furamide, AldrichCPR;Z57243693;Furan-2-carboxylic acid (4-amino-2-methyl-phenyl)-amide

Chemical Property of N-(4-amino-2-methylphenyl)furan-2-carboxamide

Chemical Property:

• Vapor Pressure: 0.00187mmHg at 25°C
• Boiling Point: 292.1°C at 760 mmHg
• Flash Point: 130.5°C
• PSA: 68.26000
• Density: 1.274g/cm³
• LogP: 3.07670
• XLogP3: 1.8
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 216.089877630
• Heavy Atom Count: 16
• Complexity: 257

Purity/Quality:

98%min ^*data from raw suppliers

N-(4-amino-2-methylphenyl)-2-furamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C=CC(=C1)N)NC(=O)C2=CC=CO2

Technology Process of N-(4-amino-2-methylphenyl)furan-2-carboxamide

There total 3 articles about N-(4-amino-2-methylphenyl)furan-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Furan-2-carboxylic acid (2-methyl-4-nitro-phenyl)-amide (200394-14-5) → Furan-2-carboxylic acid (4-amino-2-methyl-phenyl)-amide (404832-64-0)

Guidance literature:

With reducing agent; In ethanol;

DOI:10.1016/S0960-894X(03)00586-9

Reference yield:

2-furancarbonyl chloride (527-69-5) → Furan-2-carboxylic acid (4-amino-2-methyl-phenyl)-amide (404832-64-0)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / Heating

2: reducing agent / ethanol

With reducing agent; In tetrahydrofuran; ethanol;

DOI:10.1016/S0960-894X(03)00586-9

Reference yield:

2-methyl-4-nitro-benzenamine (99-52-5) → Furan-2-carboxylic acid (4-amino-2-methyl-phenyl)-amide (404832-64-0)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran / Heating

2: reducing agent / ethanol

With reducing agent; In tetrahydrofuran; ethanol;

DOI:10.1016/S0960-894X(03)00586-9

upstream raw materials:

Furan-2-carboxylic acid (2-methyl-4-nitro-phenyl)-amide

2-furancarbonyl chloride

2-methyl-4-nitro-benzenamine

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