2,3-Dioxo-3-P-tolyl-propionic acid tert-butyl ester

Base Information

Chemical Name:2,3-Dioxo-3-P-tolyl-propionic acid tert-butyl ester
CAS No.:138714-54-2
Molecular Formula:C14H16O4
Molecular Weight:248.27
Hs Code.:2918300090
DSSTox Substance ID:DTXSID901215839
Mol file:138714-54-2.mol

Synonyms:138714-54-2;2,3-DIOXO-3-P-TOLYL-PROPIONIC ACID TERT-BUTYL ESTER;TERT-BUTYL 3-(4-METHYLPHENYL)-2,3-DIOXOPROPANOATE;tert-Butyl 2,3-dioxo-3-(p-tolyl)propanoate;DTXSID901215839

Suppliers and Price of 2,3-Dioxo-3-P-tolyl-propionic acid tert-butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2,3-DIOXO-3-P-TOLYL-PROPIONIC ACID TERT-BUTYL ESTER 95.00%
5MG
$ 501.50

Total 2 raw suppliers

Chemical Property of 2,3-Dioxo-3-P-tolyl-propionic acid tert-butyl ester

Chemical Property:

PSA：60.44000
LogP:2.08850
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:248.10485899
Heavy Atom Count:18
Complexity:343

Purity/Quality:

99.0%min ^*data from raw suppliers

2,3-DIOXO-3-P-TOLYL-PROPIONIC ACID TERT-BUTYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(=O)C(=O)C(=O)OC(C)(C)C

Technology Process of 2,3-Dioxo-3-P-tolyl-propionic acid tert-butyl ester

There total 6 articles about 2,3-Dioxo-3-P-tolyl-propionic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 138714-60-0
3-Oxo-3-p-tolyl-2-(triphenyl-λ⁵-phosphanylidene)-propionic acid tert-butyl ester

: 138714-54-2
t-butyl 2,3-dioxo-3-(4-tolyl)propionate

Guidance literature:: With Oxone; In tetrahydrofuran; water; for 2h; Ambient temperature;

Reference yield:

: 86302-43-4,35000-38-5
(tert-Butoxycarbonylmethylene)triphenylphosphorane

: 138714-54-2
t-butyl 2,3-dioxo-3-(4-tolyl)propionate

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / bis(trimethylsilyl)acetamide / benzene / 2 h / 25 °C

2: 91 percent / Oxone / tetrahydrofuran; H₂O / 2 h / Ambient temperature

With Oxone; bis-(trimethylsilyl)acetamide; In tetrahydrofuran; water; benzene;

Reference yield:

: 874-60-2
4-methyl-benzoyl chloride

: 138714-54-2
t-butyl 2,3-dioxo-3-(4-tolyl)propionate

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / bis(trimethylsilyl)acetamide / benzene / 2 h / 25 °C

2: 91 percent / Oxone / tetrahydrofuran; H₂O / 2 h / Ambient temperature

With Oxone; bis-(trimethylsilyl)acetamide; In tetrahydrofuran; water; benzene;