(2S,3R,4S,5R,6R)-5-Hydroxy-2-methoxy-6-((trityloxy)methyl)tetrahydro-2H-pyran-3,4-diyl diacetate

Base Information

Chemical Name:(2S,3R,4S,5R,6R)-5-Hydroxy-2-methoxy-6-((trityloxy)methyl)tetrahydro-2H-pyran-3,4-diyl diacetate
CAS No.:53717-00-3
Molecular Formula:C₃₀H₃₂O₈
Molecular Weight:0
Hs Code.:

Synonyms:(2S,3R,4S,5R,6R)-5-Hydroxy-2-methoxy-6-((trityloxy)methyl)tetrahydro-2H-pyran-3,4-diyl diacetate

Suppliers and Price of (2S,3R,4S,5R,6R)-5-Hydroxy-2-methoxy-6-((trityloxy)methyl)tetrahydro-2H-pyran-3,4-diyl diacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 5 raw suppliers

Chemical Property of (2S,3R,4S,5R,6R)-5-Hydroxy-2-methoxy-6-((trityloxy)methyl)tetrahydro-2H-pyran-3,4-diyl diacetate

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

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Hazard Codes:

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Technology Process of (2S,3R,4S,5R,6R)-5-Hydroxy-2-methoxy-6-((trityloxy)methyl)tetrahydro-2H-pyran-3,4-diyl diacetate

There total 4 articles about (2S,3R,4S,5R,6R)-5-Hydroxy-2-methoxy-6-((trityloxy)methyl)tetrahydro-2H-pyran-3,4-diyl diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 76-84-6
triphenylmethyl alcohol

: 29868-42-6
methyl 2,3-di-O-acetyl-α-D-glucopyranoside

: 53717-00-3
methyl 2,3-di-O-acetyl-6-O-trityl-α-D-glucopyranoside

Guidance literature:: With 4 A molecular sieve; triethylamine; In toluene; at 20 ℃; for 8h;
DOI:10.1016/S0040-4039(03)00758-5

Reference yield:

: 76-83-5
trityl chloride

: 29868-42-6
methyl 2,3-di-O-acetyl-α-D-glucopyranoside

: 53717-00-3
methyl 2,3-di-O-acetyl-6-O-trityl-α-D-glucopyranoside

Guidance literature:: With pyridine;
DOI:10.1021/ja01640a065

Reference yield:

: 108-24-7
acetic anhydride

: 18311-26-7
methyl 6-O-trityl-α-D-glucopyranoside

: 53717-00-3
methyl 2,3-di-O-acetyl-6-O-trityl-α-D-glucopyranoside

: 7511-40-2,18031-49-7,31873-39-9,38982-56-8,63167-74-8,87591-35-3
methyl 2,3,4-tri-O-acetyl-6-O-trityl-α-D-glucopyranoside

Guidance literature:: With 2,3-dihydro-5,7-bismethyl-1,4-diazepine monohydroperchlorate; In neat (no solvent); at 35 - 40 ℃; for 5h; Overall yield = 95 %; regioselective reaction;
DOI:10.1039/c6ra28882k