ETHYL 3-CARBOETHOXYBENZOYLFORMATE

Base Information

• Chemical Name: ETHYL 3-CARBOETHOXYBENZOYLFORMATE
• CAS No.: 732249-84-2
• Molecular Formula: C₁₃H₁₄O₅
• Molecular Weight: 250.251
• Hs Code.: 2918990090
• Mol file: 732249-84-2.mol

Synonyms:ETHYL 3-CARBOETHOXYBENZOYLFORMATE

Chemical Property of ETHYL 3-CARBOETHOXYBENZOYLFORMATE

Chemical Property:

• Vapor Pressure: 1.25E-05mmHg at 25°C
• Boiling Point: 368.7°C at 760 mmHg
• Flash Point: 162.9°C
• PSA: 69.67000
• Density: 1.181g/cm³
• LogP: 1.60910

Purity/Quality:

95% ^*data from raw suppliers

Ethyl3-carboethoxybenzoylformate 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ETHYL 3-CARBOETHOXYBENZOYLFORMATE

There total 2 articles about ETHYL 3-CARBOETHOXYBENZOYLFORMATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-iodobenzoic acid methyl ester (58313-23-8) + oxalic acid diethyl ester (95-92-1) → ethyl 2-(3-ethoxycarbonylphenyl)-2-oxoacetate (732249-84-2)

Guidance literature:

3-iodobenzoic acid methyl ester; With phenyllithium; In diethyl ether; cyclohexane; at -60 ℃; for 1.13889E-05h; Flow reactor;

oxalic acid diethyl ester; In diethyl ether; cyclohexane; at -60 ℃; for 0.000466667h; Flow reactor;

With water; acetic acid; In tetrahydrofuran; hexane; Temperature;

DOI:10.1039/c3cc40392k

Reference yield:

→ ethyl 2-(3-ethoxycarbonylphenyl)-2-oxoacetate (732249-84-2)

Guidance literature:

Bis-homo-1,3-acetylbenzol, C2H5OH/SeO2;

upstream raw materials:

3-iodobenzoic acid methyl ester

oxalic acid diethyl ester

Refernces