1-(2-Deoxy-β-D-ribopyranosyl)thymine

Base Information

• Chemical Name: 1-(2-Deoxy-β-D-ribopyranosyl)thymine
• CAS No.: 13091-56-0
• Molecular Formula: C10H14N2O5
• Molecular Weight: 242.232
• Mol file: 13091-56-0.mol

Synonyms:1-(2-Deoxy-β-D-erythro-pentopyranosyl)-5-methyl-2,4(1H,3H)-pyrimidinedione;1-(2-Deoxy-β-D-erythro-pentopyranosyl)thymine;1-(2-Deoxy-β-D-ribopyranosyl)thymine

Chemical Property of 1-(2-Deoxy-β-D-ribopyranosyl)thymine

Chemical Property:

• PSA: 104.55000
• LogP: -1.51430

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(2-Deoxy-β-D-ribopyranosyl)thymine

There total 5 articles about 1-(2-Deoxy-β-D-ribopyranosyl)thymine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

C24H22N2O7 (155976-46-8) → 1-(2-Deoxy-β-D-erythro-pentopyranosyl)thymine (13091-56-0) + 1-(2'-Desoxy-α-D-ribopyranosyl)-thymin (13091-57-1)

Guidance literature:

With ammonia; In methanol;

DOI:10.1016/S0040-4039(00)97641-X

Reference yield: 15.1%

(5R,6R)-trans-(+)-5-bromo-6-hydroxy-5,6-dihydrothymidine (43179-29-9) → thymin (65-71-4,28806-14-6,691841-57-3) + 1-(2-Deoxy-β-D-erythro-pentopyranosyl)thymine (13091-56-0) + thymidine (50-89-5,28854-96-8,3545-96-8,50-88-4)

Guidance literature:

With copper(II) sulfate; ascorbic acid; In water; for 0.0833333h; Ambient temperature;

DOI:10.1039/c39890000238

Reference yield: 14.3%

(5S,6S)-trans-(-)-5-bromo-6-hydroxy-5,6-dihydrothymidine (43179-28-8) → thymin (65-71-4,28806-14-6,691841-57-3) + 1-(2-Deoxy-β-D-erythro-pentopyranosyl)thymine (13091-56-0) + thymidine (50-89-5,28854-96-8,3545-96-8,50-88-4)

Guidance literature:

With copper(II) sulfate; ascorbic acid; In water; for 0.0833333h; Ambient temperature;

DOI:10.1039/c39890000238

upstream raw materials:

C₂₄H₂₂N₂O₇

(5R,6R)-trans-(+)-5-bromo-6-hydroxy-5,6-dihydrothymidine

(5S,6S)-trans-(-)-5-bromo-6-hydroxy-5,6-dihydrothymidine

thymidine

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