Isoquinoline, 5-azido- (9CI)

Base Information

• Chemical Name: Isoquinoline, 5-azido- (9CI)
• CAS No.: 43101-10-6
• Molecular Formula: C9H6N4
• Molecular Weight: 170.173
• Hs Code.: 2933499090
• Mol file: 43101-10-6.mol

Synonyms:Isoquinoline, 5-azido- (9CI);5-Azidoisoquinoline

Chemical Property of Isoquinoline, 5-azido- (9CI)

Chemical Property:

• PSA: 62.64000
• LogP: 2.62936

Purity/Quality:

5-azidoisoquinoline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Isoquinoline, 5-azido- (9CI)

There total 1 articles about Isoquinoline, 5-azido- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.9%

isoquinolin-5-ylamine (1125-60-6) → 5-isoquinolyl azide (43101-10-6)

Guidance literature:

isoquinolin-5-ylamine; With sulfuric acid; In water; at 0 ℃; for 0.0833333h;

With sodium azide; In water; at 20 ℃; for 0.166667h;

Reference yield: 98.0%

1-(2-methoxyphenyl)-4-(pent-4-yn-1-yl)-piperazine + 5-isoquinolyl azide (43101-10-6) → 5-(4-(3-(4-(2-methoxyphenyl)piperazin-1-yl)propyl)-1H-1,2,3-triazol-1-yl)isoquinoline

Guidance literature:

With cerium(IV) sulphate; carbonyl(pentamethylcyclopentadienyl)cobalt diiodide; potassium acetate; silver trifluoromethanesulfonate; In nitromethane; at 100 ℃; for 36h; Schlenk technique; Inert atmosphere; Molecular sieve;

DOI:10.1002/adsc.201600025

Reference yield: 79.2%

1-(heptyn-6-yl)-4-(2-methoxyphenyl)piperazine + 5-isoquinolyl azide (43101-10-6) → 5-(4-(5-(4-(2-methoxyphenyl)piperazin-1-yl)pentyl)-1H-1,2,3-triazol-1-yl)isoquinoline

Guidance literature:

1-(heptyn-6-yl)-4-(2-methoxyphenyl)piperazine; 5-isoquinolyl azide; With copper(II) sulfate; In water; tert-butyl alcohol; for 0.25h;

With sodium L-ascorbate; In water; tert-butyl alcohol; at 60 ℃; for 8h; Inert atmosphere;

DOI:10.1016/j.bmcl.2014.12.023

upstream raw materials:

isoquinolin-5-ylamine

Downstream raw materials:

Cyclohexyl-(9H-pyrido[4,3-c]azepin-5-yl)-amine

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