(4S)-4-Phenyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester, min. 97%

Base Information

• Chemical Name: (4S)-4-Phenyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester, min. 97%
• CAS No.: 479687-23-5
• Molecular Formula: C13H17NO5S
• Molecular Weight: 299.348
• Hs Code.: 2934100090
• Mol file: 479687-23-5.mol

Synonyms:(4S)-4-Phenyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester, min. 97%;tert-butyl (4S)-2,2-dioxo-4-phenyl-1,2,3-oxathiazolidine-3-carboxylate

Chemical Property of (4S)-4-Phenyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester, min. 97%

Chemical Property:

• Sensitive.: air sensitive, store cold

Purity/Quality:

97% ^*data from raw suppliers

(4S)-4-Phenyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester, min. 97% ^*data from reagent suppliers

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Technology Process of (4S)-4-Phenyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester, min. 97%

There total 6 articles about (4S)-4-Phenyl-1,2,3-oxathiazolidine-2,2-dioxide-3-carboxylic acid t-butyl ester, min. 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

tert-butyl N-[(1S)-2-hydroxy-1-phenylethyl]carbamate (117049-14-6) → 1,2,3-oxathiazolidine-3-carboxylic acid, 4-phenyl 1,1-dimethylethyl ester-2,2-dioxide (479687-23-5)

Guidance literature:

tert-butyl N-[(1S)-2-hydroxy-1-phenylethyl]carbamate; With 1H-imidazole; thionyl chloride; triethylamine; In dichloromethane; at -60 ℃; Inert atmosphere;

With sodium periodate; ruthenium(III) trichloride hydrate; In water; acetonitrile; at 0 ℃;

DOI:10.1021/ol402988s

Reference yield: 94.0%

2-oxo-4-phenyl-2λ4-[1,2,3]oxathiazolidine-3-carboxylic acid tert-butyl ester (479687-18-8) → 1,2,3-oxathiazolidine-3-carboxylic acid, 4-phenyl 1,1-dimethylethyl ester-2,2-dioxide (479687-23-5)

Guidance literature:

With ruthenium trichloride; sodium periodate; In acetonitrile; at 0 - 20 ℃; for 1h;

DOI:10.1039/b204844b

Reference yield: 42.0%

→ 1,2,3-oxathiazolidine-3-carboxylic acid, 4-phenyl 1,1-dimethylethyl ester-2,2-dioxide (479687-23-5)

Guidance literature:

With pyridine; thionyl chloride; In dichloromethane; at -40 ℃; for 2.5h; Inert atmosphere;

With ruthenium trichloride; sodium periodate; In water; acetonitrile; at 0 - 20 ℃; for 2.25h; Inert atmosphere;

upstream raw materials:

2-oxo-4-phenyl-2λ⁴-[1,2,3]oxathiazolidine-3-carboxylic acid tert-butyl ester

di-tert-butyl dicarbonate

tert-butyl N-[(1S)-2-hydroxy-1-phenylethyl]carbamate

(2S)-2-phenylglycinol

Downstream raw materials:

{(S)-2-ethyl-[(4-nitro-benzenesulfonyl)amino]-1-phenyl-ethyl}carbamic acid tert-butyl ester

C₁₅H₂₄NO₅P

(S)-tert-butyl 2-(diethoxyphosphoryl)-1-phenylethylcarbamate

(S)-1-phenyl-2-(pyrrolidin-1-yl)ethanamine

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