S-4-oxide-8,9,10,11,12,13,14,15-octahydro-4-hydroxy-2,6-di-9-phenanthrenyl-Dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin

Base Information

• Chemical Name: S-4-oxide-8,9,10,11,12,13,14,15-octahydro-4-hydroxy-2,6-di-9-phenanthrenyl-Dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin
• CAS No.: 1028416-47-8
• Molecular Formula: C₄₈H₃₇O₄P
• Molecular Weight: 708.793
• Mol file: 1028416-47-8.mol

Synonyms:S-4-oxide-8,9,10,11,12,13,14,15-octahydro-4-hydroxy-2,6-di-9-phenanthrenyl-Dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin;(11bS) -8,9,10,11,12,13,14,15-Octahydro-4-hydroxy-2,6-di-9- phenanthrenyl-4-oxide-dinaphtho[2,1-d:1',2'-f][1,3,2] dioxaphosphepin

Chemical Property of S-4-oxide-8,9,10,11,12,13,14,15-octahydro-4-hydroxy-2,6-di-9-phenanthrenyl-Dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin

Chemical Property:

• PKA: 1.17±0.20(Predicted)
• Density: 1.40±0.1 g/cm3(Predicted)

Purity/Quality:

97% ^*data from raw suppliers

(11bS)-8,9,10,11,12,13,14,15-Octahydro-4-hydroxy-2,6-di-9-phenanthrenyl-4-oxide-dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin, 95% (99% ee) 95% (99% ee) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of S-4-oxide-8,9,10,11,12,13,14,15-octahydro-4-hydroxy-2,6-di-9-phenanthrenyl-Dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin

There total 2 articles about S-4-oxide-8,9,10,11,12,13,14,15-octahydro-4-hydroxy-2,6-di-9-phenanthrenyl-Dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

C48H38O2 (1028416-48-9,1011465-22-7) → 9-phenanthrenyl (1028416-47-8)

Guidance literature:

C₄₈H₃₈O₂; With pyridine; trichlorophosphate; at 80 ℃; for 2h;

With water; at 40 ℃; for 0.166667h;

With hydrogenchloride; at 100 ℃; for 0.0833333h; Further stages.;

DOI:10.1016/j.tet.2007.11.067

Reference yield:

C48H36ClO3P → 9-phenanthrenyl (1028416-47-8)

Guidance literature:

With hydrogenchloride; water;

DOI:10.1055/s-0029-1219528

upstream raw materials:

C₄₈H₃₈O₂

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