5-methyl-1-[4-C-[[[(4-methylphenyl) sulfonyl]oxy]methyl]-3,5-bis-O-(phenylmethyl)-Beta-D-arabinofuranosyl]-2,4(1H,3H)-Pyrimidinedione

Base Information

• Chemical Name: 5-methyl-1-[4-C-[[[(4-methylphenyl) sulfonyl]oxy]methyl]-3,5-bis-O-(phenylmethyl)-Beta-D-arabinofuranosyl]-2,4(1H,3H)-Pyrimidinedione
• CAS No.: 847666-73-3
• Molecular Formula: C₃₂H₃₄N₂O₉S
• Molecular Weight: 622.696
• Mol file: 847666-73-3.mol

Synonyms:5-methyl-1-[4-C-[[[(4-methylphenyl) sulfonyl]oxy]methyl]-3,5-bis-O-(phenylmethyl)-Beta-D-arabinofuranosyl]-2,4(1H,3H)-Pyrimidinedione

Chemical Property of 5-methyl-1-[4-C-[[[(4-methylphenyl) sulfonyl]oxy]methyl]-3,5-bis-O-(phenylmethyl)-Beta-D-arabinofuranosyl]-2,4(1H,3H)-Pyrimidinedione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-methyl-1-[4-C-[[[(4-methylphenyl) sulfonyl]oxy]methyl]-3,5-bis-O-(phenylmethyl)-Beta-D-arabinofuranosyl]-2,4(1H,3H)-Pyrimidinedione

There total 1 articles about 5-methyl-1-[4-C-[[[(4-methylphenyl) sulfonyl]oxy]methyl]-3,5-bis-O-(phenylmethyl)-Beta-D-arabinofuranosyl]-2,4(1H,3H)-Pyrimidinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C32H34N2O9SCH2SO2 → 3',5'-di-O-benzyl-5-methyl-4'-((p-toluenesulfonyloxy)methyl)-arabino-uridine (847666-73-3)

Guidance literature:

With sodium hydroxide; In ethanol; water; at 20 ℃; for 1h;

DOI:10.1002/anie.200604857

Reference yield:

3',5'-di-O-benzyl-5-methyl-4'-((p-toluenesulfonyloxy)methyl)-arabino-uridine (847666-73-3) → C18H22N2O9S

Guidance literature:

With cyclohexene; palladium dihydroxide; In ethanol; for 22h; Heating;

DOI:10.1002/anie.200604857

Reference yield:

3',5'-di-O-benzyl-5-methyl-4'-((p-toluenesulfonyloxy)methyl)-arabino-uridine (847666-73-3) + trifluoromethylsulfonic anhydride (358-23-6) → C33H33F3N2O11S2

Guidance literature:

With dmap; In pyridine; at 20 ℃; for 4h;

DOI:10.1021/ja710342q