Carbamic acid, N-[(4-methylphenyl)methylene]-, methyl ester

Base Information

Chemical Name:Carbamic acid, N-[(4-methylphenyl)methylene]-, methyl ester
CAS No.:199604-16-5
Molecular Formula:C10H11NO2
Molecular Weight:177.203
Hs Code.:
Mol file:199604-16-5.mol

Synonyms:Carbamic acid, N-[(4-methylphenyl)methylene]-, methyl ester

Suppliers and Price of Carbamic acid, N-[(4-methylphenyl)methylene]-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Carbamic acid, N-[(4-methylphenyl)methylene]-, methyl ester

Chemical Property:

PSA：38.66000
LogP:2.18030

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, N-[(4-methylphenyl)methylene]-, methyl ester

There total 1 articles about Carbamic acid, N-[(4-methylphenyl)methylene]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-87-0
4-methyl-benzaldehyde

: 199604-16-5
N-methoxycarbonyl-4-methylbenzaldimine

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / BuLi / hexane; tetrahydrofuran / 1.) 0 deg C, 10 min, 2.) r.t., 1 h

2: 77 percent / CHCl₃ / 1.5 h / Ambient temperature

With n-butyllithium; In tetrahydrofuran; hexane; chloroform;
DOI:10.1002/chem.19970031019

Reference yield: 65.0%

: 75-52-5
nitromethane

: 199604-16-5
N-methoxycarbonyl-4-methylbenzaldimine

: methyl (1R)-2-nitro-1-p-tolylethylcarbamate

Guidance literature:: With prolinol-based zinc complex; In tetrahydrofuran; at 20 ℃; for 14h;
DOI:10.1021/ol070618e

Reference yield: 30.0%

: 199604-16-5
N-methoxycarbonyl-4-methylbenzaldimine

: 108-95-2,27073-41-2
phenol

: methyl (4-hydroxyphenyl)(p-tolyl)methylcarbamate

: C₁₆H₁₇NO₃

Guidance literature:: With trichloroacetic acid; In chloroform; at 25 ℃; for 5h; regioselective reaction; Inert atmosphere;
DOI:10.1055/s-0037-1610250