4’-Methylumbelliferyl 2,3,4,-Tri-O-acetyl-6-O-trityl-β-D-glucopyranoside

Base Information

Chemical Name:4’-Methylumbelliferyl 2,3,4,-Tri-O-acetyl-6-O-trityl-β-D-glucopyranoside
CAS No.:937018-35-4
Molecular Formula:C41H38O11
Molecular Weight:706.746
Hs Code.:
Mol file:937018-35-4.mol

Synonyms:4’-Methylumbelliferyl 2,3,4,-Tri-O-acetyl-6-O-trityl-β-D-glucopyranoside;4-Methyl-7-[[2,3,4-tri-O-acetyl-6-O-(triphenylMethyl)-β-D-glucopyranosyl]oxy]-2H-1-benzopyran-2-one

Suppliers and Price of 4’-Methylumbelliferyl 2,3,4,-Tri-O-acetyl-6-O-trityl-β-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4’-Methylumbelliferyl2,3,4,-Tri-O-acetyl-6-O-trityl-β-D-glucopyranoside
25mg
$ 155.00

TRC
4’-Methylumbelliferyl2,3,4,-Tri-O-acetyl-6-O-trityl-β-D-glucopyranoside
250mg
$ 1230.00

American Custom Chemicals Corporation
4'-METHYLUMBELLIFERYL-2,3,4,-TRI-O-ACETYL-6-O-TRITYL-BETA-D-GLUCOPYRANOSIDE 95.00%
5MG
$ 501.35

Total 3 raw suppliers

Chemical Property of 4’-Methylumbelliferyl 2,3,4,-Tri-O-acetyl-6-O-trityl-β-D-glucopyranoside

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Melting Point:212-215 °C(Solv: ethanol (64-17-5))
Boiling Point:771.345°C at 760 mmHg
Flash Point:312.036°C
PSA：136.80000
Density:1.334g/cm³
LogP:6.00890

Purity/Quality:

95% ^*data from raw suppliers

4’-Methylumbelliferyl2,3,4,-Tri-O-acetyl-6-O-trityl-β-D-glucopyranoside ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 4’-Methylumbelliferyl 2,3,4,-Tri-O-acetyl-6-O-trityl-β-D-glucopyranoside (cas# 937018-35-4) is a compound useful in organic synthesis.

Technology Process of 4’-Methylumbelliferyl 2,3,4,-Tri-O-acetyl-6-O-trityl-β-D-glucopyranoside

There total 2 articles about 4’-Methylumbelliferyl 2,3,4,-Tri-O-acetyl-6-O-trityl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-methyl-7-(3,4,5-trihydroxy-6-trityloxymethyl-tetrahydro-pyran-2-yloxy)-chromen-2-one

: 108-24-7
acetic anhydride

: 937018-35-4
4-methylumbelliferyl-2,3,4-tri-O-acetyl-6-O-trityl-β-D-glucopyranoside

Guidance literature:: In pyridine; at 20 ℃; for 24h;
DOI:10.1055/s-2007-967972

Reference yield:

: 18997-57-4,39940-54-0
4-methylumbelliferyl β-D-glucopyranoside

: 937018-35-4
4-methylumbelliferyl-2,3,4-tri-O-acetyl-6-O-trityl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 5 h / 90 - 100 °C

2: 7.60 g / pyridine / 24 h / 20 °C

In pyridine;
DOI:10.1055/s-2007-967972

Reference yield:

: 937018-35-4
4-methylumbelliferyl-2,3,4-tri-O-acetyl-6-O-trityl-β-D-glucopyranoside

: 6160-80-1,84434-84-4
4-methylumbelliferyl-β-D-glucuronide

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / iodine; methanol / benzene / 24 h / 65 °C

2: 68 percent / aqueous sodium hypochlorite; TBAB; NaBr / 2,2,6,6-tetramethyl-1-piperidinyloxy; tetrabutylammonium bromide / aq. NaHCO₃; CH₂Cl₂ / 3 h / 0 °C

3: 85 percent / barium methoxide / methanol / 24 h / 0 - 5 °C

With methanol; sodium hypochlorite; tetrabutylammomium bromide; iodine; barium methoxide; sodium bromide; 2,2,6,6-tetramethyl-piperidine-N-oxyl; tetrabutylammomium bromide; In methanol; dichloromethane; sodium hydrogencarbonate; benzene;
DOI:10.1055/s-2007-967972