Benzoyl chloride, 3-(2-methylpropoxy)- (9CI)

Base Information

• Chemical Name: Benzoyl chloride, 3-(2-methylpropoxy)- (9CI)
• CAS No.: 443290-10-6
• Molecular Formula: C₁₁H₁₃ClO₂
• Molecular Weight: 212.676
• Hs Code.: 2918990090
• Mol file: 443290-10-6.mol

Synonyms:Benzoyl chloride, 3-(2-methylpropoxy)- (9CI);benzoyl chloride, 3-(2-methylpropoxy)-;3-(2-methylpropoxy)benzoyl chloride

Chemical Property of Benzoyl chloride, 3-(2-methylpropoxy)- (9CI)

Chemical Property:

• Vapor Pressure: 0.00244mmHg at 25°C
• Boiling Point: 287.7°C at 760 mmHg
• Flash Point: 107.2°C
• PSA: 26.30000
• Density: 1.12g/cm³
• LogP: 3.10040

Purity/Quality:

98%Min ^*data from raw suppliers

3-(2-methylpropoxy)benzoylchloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzoyl chloride, 3-(2-methylpropoxy)- (9CI)

There total 2 articles about Benzoyl chloride, 3-(2-methylpropoxy)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Carboxyphenol (99-06-9) → 3-isobutoxybenzoyl chloride (443290-10-6)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 90 °C

2: sodium hydroxide / methanol; tetrahydrofuran; water / 12 h / 20 °C

With potassium carbonate; sodium hydroxide; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;

DOI:10.3390/molecules24152783

Reference yield:

3-isobutoxy benzoic acid (350997-58-9) → 3-isobutoxybenzoyl chloride (443290-10-6)

Guidance literature:

With oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; for 2h; Inert atmosphere;

DOI:10.1021/jm501440q

Reference yield:

4-amino-3-isobutyloxybenzoic acid (1096330-27-6) + 3-isobutoxybenzoyl chloride (443290-10-6) → 3-isobutoxy-4-(3-isobutoxybenzamido)benzoic acid

Guidance literature:

With N,N-dimethyl-aniline; In acetone;

DOI:10.1021/jm501440q

upstream raw materials:

3-isobutoxy benzoic acid

3-Carboxyphenol

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