Dodecahydro-4,8-dihydroxy-3,6,9-tris(methylene)azuleno[4,5-b]furan-2-one

Base Information

Chemical Name:Dodecahydro-4,8-dihydroxy-3,6,9-tris(methylene)azuleno[4,5-b]furan-2-one
CAS No.:35730-79-1
Molecular Formula:C₁₅H₁₈O₄
Molecular Weight:262.306
Hs Code.:
Mol file:35730-79-1.mol

Synonyms:Dodecahydro-4,8-dihydroxy-3,6,9-tris(methylene)azuleno[4,5-b]furan-2-one

Suppliers and Price of Dodecahydro-4,8-dihydroxy-3,6,9-tris(methylene)azuleno[4,5-b]furan-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dodecahydro-4,8-dihydroxy-3,6,9-tris(methylene)azuleno[4,5-b]furan-2-one

Chemical Property:

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Technology Process of Dodecahydro-4,8-dihydroxy-3,6,9-tris(methylene)azuleno[4,5-b]furan-2-one

There total 42 articles about Dodecahydro-4,8-dihydroxy-3,6,9-tris(methylene)azuleno[4,5-b]furan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: (3aR,4S,6aR,8S,9aR,9bR)-8-((tert-butyldimethylsilyl)oxy)-4-hydroxy-3,6,9-trimethylenedecahydroazuleno[4,5-b]furan-2(9bH)-one

: 35932-46-8,89647-87-0,31565-50-1,35730-79-1
deacylcynaropicrin

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.bmcl.2019.04.004

Reference yield: 70.0%

C₂₇H₄₆O₄Si₂: C₂₇H₄₆O₄Si₂

: 35730-79-1
(±)-integrifolin

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/chem.201601275

Reference yield: 68.0%

: 1549718-88-8
(1R,3S,5R,6R,7R,8S)-8-hydroxy-3-(methoxymethoxy)-13,14,15-trimethylenedecahydroazuleno[6,7-β]furan-12-one

: 35932-46-8,89647-87-0,31565-50-1,35730-79-1
deacylcynaropicrin

Guidance literature:: With pyridinium p-toluenesulfonate; In tert-butyl alcohol; for 28h; Inert atmosphere; Reflux;
DOI:10.1016/j.bmcl.2013.12.099