C₅₂H₅₂N₂O₆Si₂

Base Information

Chemical Name:C₅₂H₅₂N₂O₆Si₂
CAS No.:1337561-03-1
Molecular Formula:C₅₂H₅₂N₂O₆Si₂
Molecular Weight:857.166
Hs Code.:

C<sub>52</sub>H<sub>52</sub>N<sub>2</sub>O<sub>6</sub>Si<sub>2</sub>

Synonyms:C₅₂H₅₂N₂O₆Si₂

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Chemical Property of C₅₂H₅₂N₂O₆Si₂

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Technology Process of C₅₂H₅₂N₂O₆Si₂

There total 3 articles about C₅₂H₅₂N₂O₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1337561-01-9
C₂₆H₂₇NO₃Si

: 1337561-02-0
C₂₆H₂₆INO₃Si

: 1337561-03-1
C₅₂H₅₂N₂O₆Si₂

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo201662n

Reference yield:

: 1337560-86-7
C₂₉H₃₂INO₅SSi

: 1337561-03-1
C₅₂H₅₂N₂O₆Si₂

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / 0.5 h / 0 °C

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / -30 - -20 °C

4: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; 2: Sonogashira coupling / 4: Sonogashira coupling;
DOI:10.1021/jo201662n

Reference yield:

: 1337560-94-7
C₂₄H₂₆INO₃Si

: 1337561-03-1
C₅₂H₅₂N₂O₆Si₂

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.33 h / -30 - -20 °C

3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; 1: Sonogashira coupling / 3: Sonogashira coupling;
DOI:10.1021/jo201662n