6-Dimethylamino-3-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-1,2,4-triazolo[3,4-f][1,2,4]triazine

Base Information

Chemical Name:6-Dimethylamino-3-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-1,2,4-triazolo[3,4-f][1,2,4]triazine
CAS No.:254440-93-2
Molecular Formula:C₃₂H₂₈N₆O₇
Molecular Weight:608.61
Hs Code.:

Synonyms:6-Dimethylamino-3-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-1,2,4-triazolo[3,4-f][1,2,4]triazine

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Chemical Property of 6-Dimethylamino-3-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-1,2,4-triazolo[3,4-f][1,2,4]triazine

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Technology Process of 6-Dimethylamino-3-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-1,2,4-triazolo[3,4-f][1,2,4]triazine

There total 12 articles about 6-Dimethylamino-3-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-1,2,4-triazolo[3,4-f][1,2,4]triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 254440-91-0
8-Chloro-6-dimethylamino-3-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-1,2,4-triazolo[3,4-f][1,2,4]triazine

: 254440-93-2
6-Dimethylamino-3-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-1,2,4-triazolo[3,4-f][1,2,4]triazine

Guidance literature:: With hydrogen; magnesium oxide; palladium on activated charcoal; In ethyl acetate; at 25 ℃; for 96h;
DOI:10.1039/a905177e

Reference yield: 55.0%

: 254440-92-1
6-Dimethylamino-8-hydrazino-3-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-1,2,4-triazolo[3,4-f][1,2,4]triazine

: 254440-93-2
6-Dimethylamino-3-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-1,2,4-triazolo[3,4-f][1,2,4]triazine

Guidance literature:: With mercury(II) oxide; In ethanol; for 1h; Heating;
DOI:10.1039/a905177e

Reference yield:

: 23316-67-8
2,3,5-tri-O-benzoyl-β-D-ribofuranosyl-1-carbonitrile

: 254440-93-2
6-Dimethylamino-3-(2',3',5'-tri-O-benzoyl-β-D-ribofuranosyl)-1,2,4-triazolo[3,4-f][1,2,4]triazine

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent / HCl; H₂O / acetic acid / 0.25 h / 100 °C

2: DCC / 1,2-dichloro-ethane / 24 h / 25 °C

3: dimethylformamide / 24 h / 60 °C

4: 62 percent / POCl₃ / 0.67 h / Heating

5: 96 percent / H₂; MgO / 5 percent Pd/C / ethyl acetate / 96 h / 25 °C

With hydrogenchloride; water; hydrogen; magnesium oxide; dicyclohexyl-carbodiimide; trichlorophosphate; palladium on activated charcoal; In acetic acid; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide; 1: Hydrolysis / 2: Substitution / 3: Acylation / 4: Substitution / 5: Hydrogenolysis;
DOI:10.1039/a905177e