1-(8-chlorodibenzo[b,f]thiepin-10-yl)-4-methylpiperazine

Base Information

• Chemical Name: 1-(8-chlorodibenzo[b,f]thiepin-10-yl)-4-methylpiperazine
• CAS No.: 22431-21-6
• Molecular Formula: C19H19 Cl N2 S
• Molecular Weight: 342.892

Synonyms:Dibenzo[b,f]thiepin,piperazine deriv.; 8-Chloro-10-(4-methylpiperazino)dibenzo[b,f]thiepine; 8-Chloro-10-(4-methylpiperazinyl)dibenzo[b,f]thiepin;Dehydrochlothepin

Chemical Property of 1-(8-chlorodibenzo[b,f]thiepin-10-yl)-4-methylpiperazine

Chemical Property:

• Vapor Pressure: 4.29E-10mmHg at 25°C
• Boiling Point: 499.1°Cat760mmHg
• Flash Point: 255.6°C
• Density: 1.275g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(8-chlorodibenzo[b,f]thiepin-10-yl)-4-methylpiperazine

There total 1 articles about 1-(8-chlorodibenzo[b,f]thiepin-10-yl)-4-methylpiperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-[2-(4-chlorophenyl)sulfanylphenyl]acetic acid (13459-62-6) → Dehydrochlothepin (22431-21-6)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorus pentoxide / 4 h / 150 °C

2: titanium(IV) isopropylate / toluene / 20 h / Inert atmosphere; Reflux

With titanium(IV) isopropylate; phosphorus pentoxide; In toluene;

DOI:10.1016/j.ejmech.2016.04.058

Reference yield: 80.0%

Dehydrochlothepin (22431-21-6) → octoclothepin (13448-22-1)

Guidance literature:

With sodium tetrahydroborate; In acetic acid; at 20 ℃; for 23h;

DOI:10.1021/jm100652h

upstream raw materials:

2-[2-(4-chlorophenyl)sulfanylphenyl]acetic acid

Downstream raw materials:

octoclothepin

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