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Technology Process of C5H5FeC5H4C3C6H5ONCO2C2H5

C5H5FeC5H4C3C6H5ONCO2C2H5

Base Information
  • Chemical Name:C5H5FeC5H4C3C6H5ONCO2C2H5
  • CAS No.:271782-87-7
  • Molecular Formula:C22H19FeNO3
  • Molecular Weight:401.245
  • Hs Code.:
C<sub>5</sub>H<sub>5</sub>FeC<sub>5</sub>H<sub>4</sub>C<sub>3</sub>C<sub>6</sub>H<sub>5</sub>ONCO<sub>2</sub>C<sub>2</sub>H<sub>5</sub>

Synonyms:C5H5FeC5H4C3C6H5ONCO2C2H5

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Chemical Property of C5H5FeC5H4C3C6H5ONCO2C2H5
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Technology Process of C5H5FeC5H4C3C6H5ONCO2C2H5

There total 1 articles about C5H5FeC5H4C3C6H5ONCO2C2H5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

tri-n-butylstannylferrocene

tri-n-butylstannylferrocene

BrC<sub>3</sub>C<sub>6</sub>H<sub>5</sub>ONCO<sub>2</sub>C<sub>2</sub>H<sub>5</sub>
269745-90-6

BrC3C6H5ONCO2C2H5

C<sub>5</sub>H<sub>5</sub>FeC<sub>5</sub>H<sub>4</sub>C<sub>3</sub>C<sub>6</sub>H<sub>5</sub>ONCO<sub>2</sub>C<sub>2</sub>H<sub>5</sub>
271782-87-7

C5H5FeC5H4C3C6H5ONCO2C2H5

Guidance literature:
With tetrakis(triphenylphosphine) palladium(0); copper(II) oxide; In N,N-dimethyl-formamide; a mixt. of heteroarene, Pd(PPh3)4 and CuO in dry DMF was heated to 130°C under Ar for 30 min, then Fc-SnBu3 was added at 100°C and heated at 120-130°C for 1.5 h; H2O was added, extd. with ether or CH2Cl2, the organic layer was washedwith satd. KF soln., water and dried over MgSO4; chromd. on silica gel column (petroleum-acetone);
DOI:10.1016/S0022-328X(99)00733-0
upstream raw materials:

BrC3C6H5ONCO2C2H5

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