(E)-4-[2-(4-(methoxy tetraethoxy)phenyl)vinyl]benzonitrile

Base Information

• Chemical Name: (E)-4-[2-(4-(methoxy tetraethoxy)phenyl)vinyl]benzonitrile
• CAS No.: 1246398-00-4
• Molecular Formula: C₂₄H₂₉NO₅
• Molecular Weight: 411.498
• Mol file: 1246398-00-4.mol

Synonyms:(E)-4-[2-(4-(methoxy tetraethoxy)phenyl)vinyl]benzonitrile

Chemical Property of (E)-4-[2-(4-(methoxy tetraethoxy)phenyl)vinyl]benzonitrile

Chemical Property:

Purity/Quality:

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Technology Process of (E)-4-[2-(4-(methoxy tetraethoxy)phenyl)vinyl]benzonitrile

There total 1 articles about (E)-4-[2-(4-(methoxy tetraethoxy)phenyl)vinyl]benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

4-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethoxy)benzaldehyde (197513-69-2) + diethyl [(4-cyanophenyl)methyl]phosphonate (1552-41-6) → (E)-4-[2-(4-(methoxy tetraethoxy)phenyl)vinyl]benzonitrile (1246398-00-4)

Guidance literature:

diethyl [(4-cyanophenyl)methyl]phosphonate; With potassium tert-butylate; In N,N-dimethyl-formamide; for 0.25h; Inert atmosphere;

4-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethoxy)benzaldehyde; In N,N-dimethyl-formamide; at 20 ℃; for 2h; Inert atmosphere;

With iodine; In toluene; Reflux; Inert atmosphere;

DOI:10.1002/anie.201001702

Reference yield: 66.0%

(E)-4-[2-(4-(methoxy tetraethoxy)phenyl)vinyl]benzonitrile (1246398-00-4) + N-Cyanoguanidine (127099-85-8,780722-26-1,461-58-5) → (E)-4-[2-(4-(methoxytetraethoxy)phenyl)vinyl]phenyl diaminotriazine (1246397-95-4)

Guidance literature:

With potassium hydroxide; In N,N-dimethyl-formamide; at 120 ℃; for 0.75h; Inert atmosphere; Microwave irradiation;

DOI:10.1002/anie.201001702

upstream raw materials:

4-(2-(2-(2-(2-methoxyethoxy)ethoxy)ethoxy)ethoxy)benzaldehyde

diethyl [(4-cyanophenyl)methyl]phosphonate

Downstream raw materials:

(E)-4-[2-(4-(methoxytetraethoxy)phenyl)vinyl]phenyl diaminotriazine