5-TRANS FLUPROSTENOL

Base Information

• Chemical Name: 5-TRANS FLUPROSTENOL
• CAS No.: 57968-83-9
• Molecular Formula: C₂₃H₂₉F₃O₆
• Molecular Weight: 458.475
• Mol file: 57968-83-9.mol

Synonyms:(5E)-7-[(1R,2R,3R,5S)-3,5-dihydroxy-2-[(1E,3R)-3-hydroxy-4-[3-(trifluoromethyl)-phenoxy]-1-butenyl]cyclopentyl]-5-heptenoic acid

Chemical Property of 5-TRANS FLUPROSTENOL

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

5-trans Fluprostenol ≥95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 5-TRANS FLUPROSTENOL

There total 3 articles about 5-TRANS FLUPROSTENOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-((E)-3-hydroxy-4-(3-(trifluoromethyl)phenoxy)but-1-enyl)-5-((Z)-7-isopropoxy-7-oxohept-2-enyl)cyclopentane-1,3-diyl dibenzoate → (Z)-7-(3,5-dihydroxy-2-((E)-3-hydroxy-4-(3-(trifluoromethyl)phenoxy)but-1-enyl)cyclopentyl)hept-5-enoic acid + fluprostenol (40666-16-8,40695-32-7,54276-17-4,54276-24-3,57968-83-9,59685-93-7)

Guidance literature:

With potassium carbonate; In methanol; at 25 ℃; for 5h; Inert atmosphere;

DOI:10.2174/157017811795371485

Reference yield:

→ (Z)-7-{(1R,3R,5S)-3,5-Dihydroxy-2-[(E)-3-hydroxy-4-(3-trifluoromethyl-phenoxy)-but-1-enyl]-cyclopentyl}-hept-5-enoic acid (40666-16-8,40695-32-7,54276-17-4,54276-24-3,57968-83-9,59685-93-7)

Guidance literature:

entspr.1.9-Lacton, KOH;

Reference yield:

2,2-bis(hydroxymethyl)propyl 7-[(1R,2R,3R,5S)-3,5-dihydroxy-2-[(1E,3R)-3-hydroxy-4-[3-(trifluoromethyl)-phenoxy]-1-butenyl]cyclopentyl]-5-heptenate → (5E)-7-[(1R,2R,3R,5S)-3,5-dihydroxy-2-[(1E,3R)-3-hydroxy-4-[3-(trifluoromethyl)-phenoxy]-1-butenyl]cyclopentyl]-5-heptenoic acid (57968-83-9) + (+)-fluprostenol (54276-17-4)

Guidance literature:

2,2-bis(hydroxymethyl)propyl 7-[(1R,2R,3R,5S)-3,5-dihydroxy-2-[(1E,3R)-3-hydroxy-4-[3-(trifluoromethyl)-phenoxy]-1-butenyl]cyclopentyl]-5-heptenate; With lithium hydroxide monohydrate; In methanol;

With citric acid; In water; pH=4 - 5; Overall yield = ~ 98 %; Overall yield = 1.43 g;

DOI:10.1016/j.tet.2012.11.087

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