Technology Process of C60H73N3O26
There total 11 articles about C60H73N3O26 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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Multi-step reaction with 5 steps
1: 75 percent / AgClO4, CpZrCl2 / CH2Cl2 / 6 h / -30 °C
2: 94 percent / HOAc, TBAF / tetrahydrofuran / 72 h / Ambient temperature
3: BF3*Et2O, 4A molecular sieves / CH2Cl2 / a) -30 deg C, overnight, b) RT, 3 h
4: pyridine / Ambient temperature
5: 99 percent / 80percent aq. AcOH / 20 - 40 °C
With
pyridine; (η(5)-cyclopentadienyl)zirconium dichloride radical; 4 A molecular sieve; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; silver perchlorate; acetic acid;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/ja980724z
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 99.8 percent / Et(i-Pr)2N, PhSH / acetonitrile / 1 h / 0 °C
2: 70 percent / K2CO3 / CH2Cl2 / 5 h / 0 - 20 °C
3: 29 percent / TMSOTf, 4A molecular sieves / CH2Cl2 / 4.5 h / -78 - 20 °C
4: 94 percent / HOAc, TBAF / tetrahydrofuran / 72 h / Ambient temperature
5: BF3*Et2O, 4A molecular sieves / CH2Cl2 / a) -30 deg C, overnight, b) RT, 3 h
6: pyridine / Ambient temperature
7: 99 percent / 80percent aq. AcOH / 20 - 40 °C
With
pyridine; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; potassium carbonate; acetic acid; thiophenol; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/ja980724z
