N-<4-(1,1-Dimethylethyl)phenylmethyl>-N,2,3-trimethyl-7-benzofurancarboxamid

Base Information

Chemical Name:N-<4-(1,1-Dimethylethyl)phenylmethyl>-N,2,3-trimethyl-7-benzofurancarboxamid
CAS No.:149530-65-4
Molecular Formula:C₂₃H₂₇NO₂
Molecular Weight:349.473
Hs Code.:

Synonyms:N-<4-(1,1-Dimethylethyl)phenylmethyl>-N,2,3-trimethyl-7-benzofurancarboxamid

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Chemical Property of N-<4-(1,1-Dimethylethyl)phenylmethyl>-N,2,3-trimethyl-7-benzofurancarboxamid

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Technology Process of N-<4-(1,1-Dimethylethyl)phenylmethyl>-N,2,3-trimethyl-7-benzofurancarboxamid

There total 3 articles about N-<4-(1,1-Dimethylethyl)phenylmethyl>-N,2,3-trimethyl-7-benzofurancarboxamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 2,3-Dihydro-N-<4-(1,1-dimethylethyl)phenylmethyl>-N,2,3-trimethyl-7-benzofurancarboxamid

: 149530-65-4
N-<4-(1,1-Dimethylethyl)phenylmethyl>-N,2,3-trimethyl-7-benzofurancarboxamid

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene; at 110 ℃; for 5h;
DOI:10.1002/ardp.19933260608

Reference yield:

: 103986-71-6
2,3-Dihydro-2,3-dimethyl-7-benzofurancarbonsaeure

: 149530-65-4
N-<4-(1,1-Dimethylethyl)phenylmethyl>-N,2,3-trimethyl-7-benzofurancarboxamid

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂ / toluene / 3 h / Heating

2: triethylamine / toluene / 1 h / Ambient temperature

3: 39 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / toluene / 5 h / 110 °C

With thionyl chloride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene;
DOI:10.1002/ardp.19933260608

Reference yield:

: 99853-95-9
2,3-Dimethyl-2,3-dihydro-benzofuran-7-carbonyl chloride

: 149530-65-4
N-<4-(1,1-Dimethylethyl)phenylmethyl>-N,2,3-trimethyl-7-benzofurancarboxamid

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / toluene / 1 h / Ambient temperature

2: 39 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / toluene / 5 h / 110 °C

With triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene;
DOI:10.1002/ardp.19933260608