4-methyl-N'-(4-phenylbutan-2-ylidene)benzenesulfonohydrazide

Base Information

• Chemical Name: 4-methyl-N'-(4-phenylbutan-2-ylidene)benzenesulfonohydrazide
• CAS No.: 64884-77-1
• Molecular Formula: C₁₇H₂₀N₂O₂S
• Molecular Weight: 316.424
• Mol file: 64884-77-1.mol

Synonyms:4-methyl-N'-(4-phenylbutan-2-ylidene)benzenesulfonohydrazide

Chemical Property of 4-methyl-N'-(4-phenylbutan-2-ylidene)benzenesulfonohydrazide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 4-methyl-N'-(4-phenylbutan-2-ylidene)benzenesulfonohydrazide

There total 1 articles about 4-methyl-N'-(4-phenylbutan-2-ylidene)benzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.5%

4-Phenyl-2-butanone (2550-26-7) + toluene-4-sulfonic acid hydrazide (1576-35-8) → 4-methyl-N'-(4-phenylbutan-2-ylidene)benzenesulfonohydrazide (64884-77-1)

Guidance literature:

In methanol; at 20 ℃; Inert atmosphere;

DOI:10.1021/ol5011714

Reference yield: 100.0%

4-methyl-N'-(4-phenylbutan-2-ylidene)benzenesulfonohydrazide (64884-77-1) → 4-Phenyl-2-butanone (2550-26-7)

Guidance literature:

With copper(II) sulfate; In tetrahydrofuran; methanol; water; for 3h; Heating;

Reference yield: 80.0%

triethylsilane (617-86-7) + 4-methyl-N'-(4-phenylbutan-2-ylidene)benzenesulfonohydrazide (64884-77-1) → triethyl(4-phenylbutan-2-yl)silane

Guidance literature:

With bis(tri-t-butylphosphine)palladium⁽⁰⁾; lithium tert-butoxide; In 1,4-dioxane; at 120 ℃; for 2h; Inert atmosphere;

DOI:10.1039/c8cc06768f

upstream raw materials:

4-Phenyl-2-butanone

toluene-4-sulfonic acid hydrazide

Downstream raw materials:

4-Phenyl-2-butanone

p-toluenesulfonyl chloride

(1S,2S)-3-Methyl-3-phenethyl-cyclopropane-1,2-dicarboxylic acid diethyl ester

1-(4-phenylbutan-2-yl)-1H-imidazole