cis/trans-1-[4-(2-propyn-1-yloxy)cyclohexyl]-4-piperidinamine dihydrochloride

Base Information

Chemical Name:cis/trans-1-[4-(2-propyn-1-yloxy)cyclohexyl]-4-piperidinamine dihydrochloride
CAS No.:950817-66-0
Molecular Formula:C₁₄H₂₄N₂O
Molecular Weight:236.357
Hs Code.:

Synonyms:cis/trans-1-[4-(2-propyn-1-yloxy)cyclohexyl]-4-piperidinamine dihydrochloride

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Chemical Property of cis/trans-1-[4-(2-propyn-1-yloxy)cyclohexyl]-4-piperidinamine dihydrochloride

Chemical Property:

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Technology Process of cis/trans-1-[4-(2-propyn-1-yloxy)cyclohexyl]-4-piperidinamine dihydrochloride

There total 1 articles about cis/trans-1-[4-(2-propyn-1-yloxy)cyclohexyl]-4-piperidinamine dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 950772-88-0
cis/trans-1,1-dimethylethyl {1-[4-(2-propyn-1-yloxy)cyclohexyl]-4-piperidinyl}carbamate

: 950817-66-0
cis/trans-1-[4-(2-propyn-1-yloxy)cyclohexyl]-4-piperidinamine dihydrochloride

Guidance literature:: With hydrogenchloride; In ethanol; for 2h;

Reference yield:

: 950817-66-0
cis/trans-1-[4-(2-propyn-1-yloxy)cyclohexyl]-4-piperidinamine dihydrochloride

: 446-34-4
2-fluoro-4-methyl-1-nitrobenzene

: 950772-90-4
N-(5-methyl-2-nitrophenyl)-1-[trans-4-(2-propyn-1-yloxy)cyclohexyl]-4-piperidinamine

: 950772-91-5
N-(5-methyl-2-nitrophenyl)-1-[cis-4-(2-propyn-1-yloxy)cyclohexyl]-4-piperidinamine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 200 ℃; for 0.333333h; Microwave reactor;

Reference yield:

: 950817-66-0
cis/trans-1-[4-(2-propyn-1-yloxy)cyclohexyl]-4-piperidinamine dihydrochloride

: 6-methyl-1-{1-[trans-4-(2-propyn-1-yloxy)cyclohexyl]-4-piperidinyl}-1,3-dihydro-2H-benzimidazol-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.33 h / 200 °C / Microwave reactor

2: hydrogenchloride; tin(ll) chloride / ethanol; water / 0.58 h / 60 °C

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; tin(ll) chloride; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;