C₃₁H₄₀O₃Si

Base Information

Chemical Name:C₃₁H₄₀O₃Si
CAS No.:1427031-86-4
Molecular Formula:C₃₁H₄₀O₃Si
Molecular Weight:488.742
Hs Code.:

C<sub>31</sub>H<sub>40</sub>O<sub>3</sub>Si

Synonyms:C₃₁H₄₀O₃Si

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Chemical Property of C₃₁H₄₀O₃Si

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Technology Process of C₃₁H₄₀O₃Si

There total 1 articles about C₃₁H₄₀O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 127793-68-4
(S)-1-(tert-butyldiphenylsiloxy)-4-hydroxyhept-6-ene

: 89238-99-3
O-(4-methoxybenzyl)-trichloroacetimidate

: 1427031-86-4
C₃₁H₄₀O₃Si

Guidance literature:: With scandium tris(trifluoromethanesulfonate); In toluene; at 20 ℃; for 0.333333h;
DOI:10.1021/ol400408w

Reference yield:

: 1427031-86-4
C₃₁H₄₀O₃Si

: C₃₁H₄₂O₅Si

Guidance literature:: With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In tetrahydrofuran; water; tert-butyl alcohol; at 20 ℃;
DOI:10.1021/ol400408w

Reference yield:

: 1427031-86-4
C₃₁H₄₀O₃Si

: 1427032-08-3
C₃₃H₅₄O₈Si

Guidance literature:: Multi-step reaction with 12 steps

1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / tetrahydrofuran; water; tert-butyl alcohol / 20 °C

2: sodium periodate / tetrahydrofuran; water / 1 h / 20 °C

3: toluene / 1.33 h / -78 - 20 °C / Molecular sieve

4: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C

5: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.5 h / 0 - 20 °C / pH 7

6: diethylazodicarboxylate; triphenylphosphine / toluene; tetrahydrofuran / 2 h / 0 - 20 °C

7: diisobutylaluminium hydride / dichloromethane; hexane / 1 h / -78 °C

8: dmap / toluene / 1.5 h / 20 °C

9: Hoveyda-Grubbs catalyst second generation; p-benzoquinone / toluene / 140 °C

10: palladium 10% on activated carbon; hydrogen / methanol / 25 h / 20 °C

11: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 47 h / 20 °C

12: Dess-Martin periodane / dichloromethane / 0.5 h / 0 - 20 °C

With 2,6-dimethylpyridine; dmap; sodium periodate; osmium(VIII) oxide; Hoveyda-Grubbs catalyst second generation; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; diisobutylaluminium hydride; Dess-Martin periodane; acetic acid; 4-methylmorpholine N-oxide; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; p-benzoquinone; diethylazodicarboxylate; In tetrahydrofuran; methanol; hexane; dichloromethane; water; toluene; tert-butyl alcohol; 6: |Mitsunobu Displacement;
DOI:10.1021/ol400408w