Technology Process of C41H58O6Si
There total 7 articles about C41H58O6Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid;
In
ethanol; chloroform;
at 0 - 20 ℃;
DOI:10.1021/ol990884v
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrogen / Pd/C / ethyl acetate / 20 °C
2: 83 percent / p-toluenesulfonic acid / ethanol; CHCl3 / 0 - 20 °C
With
hydrogen; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
ethanol; chloroform; ethyl acetate;
DOI:10.1021/ol990884v
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: 92 percent / NaIO4; RuCl3; phosphate buffer / acetonitrile / 20 °C / pH 8
2.1: Me2AlCl / CH2Cl2 / 0 - 20 °C
3.1: imidazole; 4-(dimethylamino)pyridine / dimethylformamide / 0 - 20 °C
4.1: 94 percent / acetic anhydride / 20 °C
5.1: n-butyllithium / tetrahydrofuran
5.2: tetrahydrofuran
6.1: hydrogen / Pd/C / ethyl acetate / 20 °C
7.1: 83 percent / p-toluenesulfonic acid / ethanol; CHCl3 / 0 - 20 °C
With
1H-imidazole; dmap; ruthenium trichloride; sodium periodate; n-butyllithium; phosphate buffer; hydrogen; dimethylaluminum chloride; acetic anhydride; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; dichloromethane; chloroform; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol990884v