N-cyclopropylmethyl-10,11-dihydro-5H-dibenzo-(a,d)-cyclohepten-5-imine

Base Information

Chemical Name:N-cyclopropylmethyl-10,11-dihydro-5H-dibenzo-(a,d)-cyclohepten-5-imine
CAS No.:59864-46-9
Molecular Formula:C₁₉H₁₉N
Molecular Weight:261.367
Hs Code.:
Mol file:59864-46-9.mol

Synonyms:N-cyclopropylmethyl-10,11-dihydro-5H-dibenzo-(a,d)-cyclohepten-5-imine

Suppliers and Price of N-cyclopropylmethyl-10,11-dihydro-5H-dibenzo-(a,d)-cyclohepten-5-imine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of N-cyclopropylmethyl-10,11-dihydro-5H-dibenzo-(a,d)-cyclohepten-5-imine

Chemical Property:

Vapor Pressure:8.15E-06mmHg at 25°C
Boiling Point:386°C at 760 mmHg
Flash Point:179.6°C
PSA：12.36000
Density:1.14g/cm³
LogP:4.03260

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-cyclopropylmethyl-10,11-dihydro-5H-dibenzo-(a,d)-cyclohepten-5-imine

There total 3 articles about N-cyclopropylmethyl-10,11-dihydro-5H-dibenzo-(a,d)-cyclohepten-5-imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 59864-51-6
N-methyl-10,11-dihydro-5H-dibenzocyclohepten-5-imine

: 2516-47-4
cyclopropanemethylamine

: 59864-46-9
N-(cyclopropylmethyl)-10,11-dihydro-5H-dibenzocyclohepten-5-imine

Guidance literature:: With toluene-4-sulfonic acid; at 120 ℃; for 90h;
DOI:10.1021/jm00135a018

Reference yield:

: 1210-35-1
10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-one

: 59864-46-9
N-(cyclopropylmethyl)-10,11-dihydro-5H-dibenzocyclohepten-5-imine

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / TiCl₄ / benzene / 288 h / Ambient temperature

2: 65 percent / p-toluenesulfonic acid hydrate / 90 h / 120 °C

With titanium tetrachloride; toluene-4-sulfonic acid; In benzene;
DOI:10.1021/jm00135a018