2-(2-bromo-6-heptadec-10-enyl-3-hydroxy-phenoxy)-N-methoxy-N-methyl-propionamide

Base Information

Chemical Name:2-(2-bromo-6-heptadec-10-enyl-3-hydroxy-phenoxy)-N-methoxy-N-methyl-propionamide
CAS No.:903522-40-7
Molecular Formula:C₂₈H₄₆BrNO₄
Molecular Weight:540.582
Hs Code.:

2-(2-bromo-6-heptadec-10-enyl-3-hydroxy-phenoxy)-<i>N</i>-methoxy-<i>N</i>-methyl-propionamide

Synonyms:2-(2-bromo-6-heptadec-10-enyl-3-hydroxy-phenoxy)-N-methoxy-N-methyl-propionamide

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Chemical Property of 2-(2-bromo-6-heptadec-10-enyl-3-hydroxy-phenoxy)-N-methoxy-N-methyl-propionamide

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Technology Process of 2-(2-bromo-6-heptadec-10-enyl-3-hydroxy-phenoxy)-N-methoxy-N-methyl-propionamide

There total 9 articles about 2-(2-bromo-6-heptadec-10-enyl-3-hydroxy-phenoxy)-N-methoxy-N-methyl-propionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 2,2-Dimethyl-propionic acid 2-bromo-4-((Z)-heptadec-10-enyl)-3-[(S)-1-(methoxy-methyl-carbamoyl)-ethoxy]-phenyl ester

: 903522-40-7
2-(2-bromo-6-heptadec-10-enyl-3-hydroxy-phenoxy)-N-methoxy-N-methyl-propionamide

Guidance literature:: With nitromethane; zinc dibromide; at 20 ℃;
DOI:10.1021/ol061000s

Reference yield:

: 903522-39-4
Toluene-4-sulfonic acid (R)-1-(methoxy-methyl-carbamoyl)-ethyl ester

: 903522-40-7
2-(2-bromo-6-heptadec-10-enyl-3-hydroxy-phenoxy)-N-methoxy-N-methyl-propionamide

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / K₂CO₃ / dimethylformamide / 6 h / 20 °C

2: 93 percent / ZnBr; CH₃NO₂ / 20 °C

With nitromethane; potassium carbonate; zinc dibromide; In N,N-dimethyl-formamide;
DOI:10.1021/ol061000s

Reference yield:

: 2,2-dimethyl-propionic acid 2-bromo-3-(2,2-dimethyl-propionyloxy)-6-formyl-phenyl ester

: 903522-40-7
2-(2-bromo-6-heptadec-10-enyl-3-hydroxy-phenoxy)-N-methoxy-N-methyl-propionamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaBH₄ / tetrahydrofuran; H₂O

2.1: Mg / tetrahydrofuran / 4 h / Heating

2.2: 0.920 g / NaH / diethyl ether / 1.5 h / 0 - 20 °C

3.1: 92 percent / K₂CO₃ / dimethylformamide / 6 h / 20 °C

4.1: 93 percent / ZnBr; CH₃NO₂ / 20 °C

With sodium tetrahydroborate; nitromethane; potassium carbonate; magnesium; zinc dibromide; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/ol061000s