7-Amino-3-(2,5-dimethoxyphenacyl)-1-methylpyrimido-(4,5-c)pyridazine-4,5(1H, 6H)-dione

Base Information

• Chemical Name: 7-Amino-3-(2,5-dimethoxyphenacyl)-1-methylpyrimido-(4,5-c)pyridazine-4,5(1H, 6H)-dione
• CAS No.: 80081-82-9
• Molecular Formula: C₁₇H₁₇N₅O₅
• Molecular Weight: 371.352

Synonyms:7-Amino-3-(2,5-dimethoxyphenacyl)-1-methylpyrimido-(4,5-c)pyridazine-4,5(1H, 6H)-dione

Chemical Property of 7-Amino-3-(2,5-dimethoxyphenacyl)-1-methylpyrimido-(4,5-c)pyridazine-4,5(1H, 6H)-dione

Chemical Property:

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Technology Process of 7-Amino-3-(2,5-dimethoxyphenacyl)-1-methylpyrimido-(4,5-c)pyridazine-4,5(1H, 6H)-dione

There total 3 articles about 7-Amino-3-(2,5-dimethoxyphenacyl)-1-methylpyrimido-(4,5-c)pyridazine-4,5(1H, 6H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-(1-methylhydrazino)isocytosine hemihydrate + methyl 2,5-dimethoxybenzoylpyruvate (70935-15-8) → 7-Amino-3-(2,5-dimethoxyphenacyl)-1-methylpyrimido-(4,5-c)pyridazine-4,5(1H, 6H)-dione (80081-82-9)

Guidance literature:

In methanol;

Reference yield:

methyl 2,5-dimethoxybenzoylpyruvate (70935-15-8) + 2-amino-6-(1-methylhydrazinyl)pyrimidin-4(3H)-one (67873-21-6) → 7-Amino-3-(2,5-dimethoxyphenacyl)-1-methylpyrimido-(4,5-c)pyridazine-4,5(1H, 6H)-dione (80081-82-9) + 7-Amino-4-[2-(2,5-dimethoxy-phenyl)-2-oxo-ethyl]-1-methyl-1,2-dihydro-pyrimido[4,5-c]pyridazine-3,5-dione (80081-77-2) + 8-Amino-5-(2,5-dimethoxy-phenyl)-1-methyl-6-oxo-6,7-dihydro-1H-pyrimido[4,5-c][1,2]diazepine-3-carboxylic acid methyl ester (80081-87-4)

Guidance literature:

In methanol; for 49h; Yields of byproduct given; Heating;

DOI:10.1021/jo00343a013

Reference yield:

methyl 2,5-dimethoxybenzoylpyruvate (70935-15-8) + 2-amino-6-(1-methylhydrazinyl)pyrimidin-4(3H)-one (67873-21-6) → 7-Amino-3-(2,5-dimethoxyphenacyl)-1-methylpyrimido-(4,5-c)pyridazine-4,5(1H, 6H)-dione (80081-82-9) + 7-Amino-4-[2-(2,5-dimethoxy-phenyl)-2-oxo-ethyl]-1-methyl-1,2-dihydro-pyrimido[4,5-c]pyridazine-3,5-dione (80081-77-2)

Guidance literature:

In methanol; for 42.5h; Yield given; Heating;

DOI:10.1021/jo00343a013

upstream raw materials:

methyl 2,5-dimethoxybenzoylpyruvate

2-amino-6-(1-methylhydrazinyl)pyrimidin-4(3H)-one

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