mer-{FeI(1,2-bis(diphenylphosphino)methane)(phenyl isocyanide)3}I

Base Information

Chemical Name:mer-{FeI(1,2-bis(diphenylphosphino)methane)(phenyl isocyanide)3}I
CAS No.:95402-11-2
Molecular Formula:C₄₆H₃₇FeIN₃P₂*I
Molecular Weight:1003.42
Hs Code.:

Synonyms:mer-{FeI(1,2-bis(diphenylphosphino)methane)(phenyl isocyanide)3}I

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Chemical Property of mer-{FeI(1,2-bis(diphenylphosphino)methane)(phenyl isocyanide)3}I

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Technology Process of mer-{FeI(1,2-bis(diphenylphosphino)methane)(phenyl isocyanide)3}I

There total 2 articles about mer-{FeI(1,2-bis(diphenylphosphino)methane)(phenyl isocyanide)3}I which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 137679-82-4,137766-34-8
I₂Fe(C₆H₅NC)4

: 2071-20-7
bis-diphenylphosphinomethane

: 95402-11-2
mer-{FeI(1,2-bis(diphenylphosphino)methane)(phenyl isocyanide)3}I

Guidance literature:: In toluene; under Ar, toluene soln. of educts refluxed for 1 h; ppt. filtered, washed with diethyl ether, recrystd. from CH2Cl2/EtOH, elem. anal.;
DOI:10.1016/0022-328X(84)80603-8

Reference yield:

: {Fe((C₆H₅)2PCHP(C₆H₅)2)(C₆H₅NC)3I}

: 95402-11-2
mer-{FeI(1,2-bis(diphenylphosphino)methane)(phenyl isocyanide)3}I

Guidance literature:: With H(+); (Me₃O)SbCl₆; treating with weak acid;

Reference yield: 95.0%

: 95402-11-2
mer-{FeI(1,2-bis(diphenylphosphino)methane)(phenyl isocyanide)3}I

: {Fe((C₆H₅)2PCHP(C₆H₅)2)(C₆H₅NC)3I}

Guidance literature:: With KOH; In dichloromethane; to a soln. of iron complex an excess of KOH is added, stirring for 4 h (under Ar); filtn. under Ar, evapn., residue is washed and stirred with Et2O, recrystd. from pyridine-Et2O, elem. anal.;