tert-butyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinate

Base Information

• Chemical Name: tert-butyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinate
• CAS No.: 1022160-19-5
• Molecular Formula: C₄₇H₅₈N₄O₉
• Molecular Weight: 822.999

Synonyms:tert-butyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinate

Chemical Property of tert-butyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinate

Chemical Property:

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Technology Process of tert-butyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinate

There total 1 articles about tert-butyl N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

N5-acetyl-N5-benzyloxy-N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithine (1022160-15-1) + glycine tert-butyl ester hydrochloride (27532-96-3) → tert-butyl N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N5-acetyl-N5-benzyloxy-L-ornithinyl-glycinate (1022160-19-5)

Guidance literature:

With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃;

DOI:10.1016/j.tetlet.2008.02.007

Reference yield: 92.0%

tert-butyl N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N5-acetyl-N5-benzyloxy-L-ornithinyl-glycinate (1022160-19-5) → N2-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N5-acetyl-N5-benzyloxy-L-ornithinyl-glycine (1022160-17-3)

Guidance literature:

With trifluoroacetic acid; In dichloromethane;

DOI:10.1016/j.tetlet.2008.02.007

upstream raw materials:

N⁵-acetyl-N⁵-benzyloxy-N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-L-ornithine

glycine tert-butyl ester hydrochloride

Downstream raw materials:

N²-(2,3-dibenzyloxybenzoyl)aminohexanoylcarbonyl-N⁵-acetyl-N⁵-benzyloxy-L-ornithinyl-glycine

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