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Technology Process of (C6H5C5HN)4ZnH3C6H4CCH

(C6H5C5HN)4ZnH3C6H4CCH

Base Information
  • Chemical Name:(C6H5C5HN)4ZnH3C6H4CCH
  • CAS No.:1227063-63-9
  • Molecular Formula:C52H32N4Zn
  • Molecular Weight:778.243
  • Hs Code.:
(C<sub>6</sub>H<sub>5</sub>C<sub>5</sub>HN)4ZnH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>CCH

Synonyms:(C6H5C5HN)4ZnH3C6H4CCH

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Chemical Property of (C6H5C5HN)4ZnH3C6H4CCH
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Technology Process of (C6H5C5HN)4ZnH3C6H4CCH

There total 2 articles about (C6H5C5HN)4ZnH3C6H4CCH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C<sub>55</sub>H<sub>40</sub>N<sub>4</sub>SiZn

C55H40N4SiZn

(C<sub>6</sub>H<sub>5</sub>C<sub>5</sub>HN)4ZnH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>CCH
1227063-63-9

(C6H5C5HN)4ZnH3C6H4CCH

Guidance literature:
With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1246/cl.2010.252

Reference yield: 99.0%

(C<sub>6</sub>H<sub>5</sub>C<sub>5</sub>HN)4ZnH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>CCSi(CH(CH<sub>3</sub>)2)3
1227063-62-8

(C6H5C5HN)4ZnH3C6H4CCSi(CH(CH3)2)3

(C<sub>6</sub>H<sub>5</sub>C<sub>5</sub>HN)4ZnH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>CCH
1227063-63-9

(C6H5C5HN)4ZnH3C6H4CCH

Guidance literature:
With Bu4NF; In not given; deprotection of Zn deriv. with Bu4NF;
DOI:10.1246/cl.2010.252

Reference yield: 81.0%

ethyl-2-azidoacetate
637-81-0

ethyl-2-azidoacetate

(C<sub>6</sub>H<sub>5</sub>C<sub>5</sub>HN)4ZnH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>CCH
1227063-63-9

(C6H5C5HN)4ZnH3C6H4CCH

(C<sub>6</sub>H<sub>5</sub>C<sub>5</sub>HN)4ZnH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>C<sub>2</sub>HN<sub>3</sub>CO<sub>2</sub>C<sub>2</sub>H<sub>5</sub>

(C6H5C5HN)4ZnH3C6H4C2HN3CO2C2H5

Guidance literature:
With copper(l) iodide; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1246/cl.2010.252
upstream raw materials:

(C6H5C5HN)4ZnH3C6H4CCSi(CH(CH3)2)3

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