C₁₈H₁₇I

Base Information

• Chemical Name: C₁₈H₁₇I
• CAS No.: 1415694-09-5
• Molecular Formula: C₁₈H₁₇I
• Molecular Weight: 360.237
• Mol file: 1415694-09-5.mol

Synonyms:C₁₈H₁₇I

Chemical Property of C₁₈H₁₇I

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of C₁₈H₁₇I

There total 1 articles about C₁₈H₁₇I which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Bromo-2-iodobenzene (583-55-1) + (4-butylphenyl)acetylene (79887-09-5) → C18H17I (1415694-09-5)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; triethylamine; In N,N-dimethyl-formamide; at 25 ℃; for 0.5h; Inert atmosphere; Sealed tube;

DOI:10.1002/asia.201601085

Reference yield: 55.0%

2-Methyl-4-phenyl-3-butyn-2-ol (1719-19-3) + C18H17I (1415694-09-5) → 3-(4-butylphenyl)-1,1-dimethyl-8-phenyl-1H-indeno[1,2-c]furan (1415694-23-3)

Guidance literature:

With palladium diacetate; magnesium sulfate; potassium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 12h; Inert atmosphere;

DOI:10.1021/jo302223y

Reference yield:

C18H17I (1415694-09-5) + (4-butylphenyl)acetylene (79887-09-5) → 1,2-bis((4-butylphenyl)ethynyl)benzene

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; triethylamine; In N,N-dimethyl-formamide; at 80 ℃; for 2h; Inert atmosphere; Sealed tube;

DOI:10.1002/asia.201601085

upstream raw materials:

1-Bromo-2-iodobenzene

(4-butylphenyl)acetylene

Downstream raw materials:

3-(4-butylphenyl)-1,1-dimethyl-8-phenyl-1H-indeno[1,2-c]furan