4-methoxy-N-(4-oxocyclohexa-2,5-dienylidene)benzenamine oxide

Base Information

• Chemical Name: 4-methoxy-N-(4-oxocyclohexa-2,5-dienylidene)benzenamine oxide
• CAS No.: 6995-98-8
• Molecular Formula: C₁₃H₁₁NO₃
• Molecular Weight: 229.235
• Mol file: 6995-98-8.mol

Synonyms:4-methoxy-N-(4-oxocyclohexa-2,5-dienylidene)benzenamine oxide

Chemical Property of 4-methoxy-N-(4-oxocyclohexa-2,5-dienylidene)benzenamine oxide

Chemical Property:

Purity/Quality:

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Technology Process of 4-methoxy-N-(4-oxocyclohexa-2,5-dienylidene)benzenamine oxide

There total 8 articles about 4-methoxy-N-(4-oxocyclohexa-2,5-dienylidene)benzenamine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

N,N'-bis(4-methoxyphenyl)-p-benzoquinone di-imine N,N'-dioxide (83925-66-0) → 4-methoxy-N-(4-oxocyclohexa-2,5-dienylidene)benzenamine oxide (6995-98-8) + 2,5-bis(4-methoxyphenylamino)-p-benzoquinone (24605-58-1) + p-benzoquinone (106-51-4) + (E)-1,2-bis(4-methoxyphenyl)diazene (501-58-6,21650-55-5,82570-64-7)

Guidance literature:

In benzene; at 20 ℃; for 6h; Irradiation;

DOI:10.1039/P19820002023

Reference yield:

bis(4-methoxyphenyl)oxoammonium perchlorate → bis(4-methoxyphenyl)nitroxyl (2643-00-7) + 4-methoxy-N-(4-oxocyclohexa-2,5-dienylidene)benzenamine oxide (6995-98-8)

Guidance literature:

With water; potassium hydroxide; In acetonitrile; at 20 ℃; for 0.333333h;

DOI:10.1134/S1070428011090090

Reference yield:

bis(4-methoxyphenyl)oxoammonium perchlorate → 4-methoxy-N-(4-oxocyclohexa-2,5-dienylidene)benzenamine oxide (6995-98-8)

Guidance literature:

With water; potassium hydroxide; at 20 ℃; for 0.333333h;

DOI:10.1134/S1070428011090090

upstream raw materials:

N,N'-bis(4-methoxyphenyl)-p-benzoquinone di-imine N,N'-dioxide

water

Downstream raw materials:

4-((4-methoxyphenyl)imino)cyclohexa-2,5-dien-1-one