2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1->4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

Base Information

Chemical Name:2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1->4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate
CAS No.:1240486-78-5
Molecular Formula:C₅₆H₇₄Cl₃NO₁₄
Molecular Weight:1091.56
Hs Code.:

2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1->4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

Synonyms:2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1->4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

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Chemical Property of 2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1->4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

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Technology Process of 2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1->4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

There total 1 articles about 2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1->4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₄H₇₄O₁₄

: 545-06-2
trichloroacetonitrile

: 1240486-78-5
2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1->4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo101231r

Reference yield: 94.0%

: 1240486-78-5
2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1->4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

: 1448686-78-9
allyl 2-O-levulinoyl-3-O-p-methoxybenzyl-α-L-rhamnopyranoside

: 1448686-79-0
allyl 2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1→4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl-(1→4)-2-O-levulinoyl-3-O-pmethoxybenzyl-α-L-rhamnopyranoside

Guidance literature:: 2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1->4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate; allyl 2-O-levulinoyl-3-O-p-methoxybenzyl-α-L-rhamnopyranoside; In dichloromethane; at 20 ℃; for 0.166667h; Molecular sieve;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 - 0 ℃; for 1.5h; Molecular sieve;
DOI:10.1021/ol4020255

Reference yield: 82.0%

: 1240486-78-5
2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1->4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate

: 1240486-77-4
C₆₀H₈₂O₁₅

: 1240486-98-9
C₁₁₄H₁₅₄O₂₈

Guidance literature:: C₆₀H₈₂O₁₅; With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 - 20 ℃; Molecular sieve; Inert atmosphere;

2-O-trans-cinnamoyl-3-O-p-methoxybenzyl-4-O-n-dodecanoyl-α-L-rhamnopyranosyl-(1->4)-2-O-2(S)-methylbutyryl-3-O-p-methoxybenzyl-α-L-rhamnopyranosyl trichloroacetimidate; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/jo101231r