5-acetamido-11,17,23-tris[3-(4-methylphenyl)ureido]-25,26,27-tripropoxy-28-(carboxymethoxy)calix[4]arene

Base Information

• Chemical Name: 5-acetamido-11,17,23-tris[3-(4-methylphenyl)ureido]-25,26,27-tripropoxy-28-(carboxymethoxy)calix[4]arene
• CAS No.: 1015191-90-8
• Molecular Formula: C₆₅H₇₁N₇O₁₀
• Molecular Weight: 1110.32
• Mol file: 1015191-90-8.mol

Synonyms:5-acetamido-11,17,23-tris[3-(4-methylphenyl)ureido]-25,26,27-tripropoxy-28-(carboxymethoxy)calix[4]arene

Chemical Property of 5-acetamido-11,17,23-tris[3-(4-methylphenyl)ureido]-25,26,27-tripropoxy-28-(carboxymethoxy)calix[4]arene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5-acetamido-11,17,23-tris[3-(4-methylphenyl)ureido]-25,26,27-tripropoxy-28-(carboxymethoxy)calix[4]arene

There total 1 articles about 5-acetamido-11,17,23-tris[3-(4-methylphenyl)ureido]-25,26,27-tripropoxy-28-(carboxymethoxy)calix[4]arene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

5-acetamido-11,17,23-tris[3-(4-methylphenyl)ureido]-25,26,27-tripropoxy-28-[(ethoxycarbonyl)methoxy]calix[4]arene (1015191-82-8) → 5-acetamido-11,17,23-tris[3-(4-methylphenyl)ureido]-25,26,27-tripropoxy-28-(carboxymethoxy)calix[4]arene (1015191-90-8)

Guidance literature:

With sodium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; for 12h;

DOI:10.1055/s-2008-1032155

Reference yield: 85.0%

5-acetamido-11,17,23-tris[3-(4-methylphenyl)ureido]-25,26,27-tripropoxy-28-(carboxymethoxy)calix[4]arene (1015191-90-8) + C2HF3O2*C115H159N9O16 (1035886-49-7) → C180H228N16O25 (1035886-51-1)

Guidance literature:

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

DOI:10.1039/b803519a

Reference yield: 80.0%

C79H95N9O8 + 5-acetamido-11,17,23-tris[3-(4-methylphenyl)ureido]-25,26,27-tripropoxy-28-(carboxymethoxy)calix[4]arene (1015191-90-8) → C144H164N16O17 (1035886-53-3)

Guidance literature:

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

DOI:10.1039/b803519a

upstream raw materials:

5-acetamido-11,17,23-tris[3-(4-methylphenyl)ureido]-25,26,27-tripropoxy-28-[(ethoxycarbonyl)methoxy]calix[4]arene

Downstream raw materials:

C₁₄₄H₁₆₄N₁₆O₁₇

C₁₈₀H₂₂₈N₁₆O₂₅

C₇₈H₉₆N₈O₁₁