t-butyl DL-3-{[(1,4-dichloro-7-isoquinolinyl)carbonyl]amino}-3-phenylpropanoate

Base Information

Chemical Name:t-butyl DL-3-{[(1,4-dichloro-7-isoquinolinyl)carbonyl]amino}-3-phenylpropanoate
CAS No.:256477-88-0
Molecular Formula:C₂₃H₂₂Cl₂N₂O₃
Molecular Weight:445.345
Hs Code.:

Synonyms:t-butyl DL-3-{[(1,4-dichloro-7-isoquinolinyl)carbonyl]amino}-3-phenylpropanoate

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Chemical Property of t-butyl DL-3-{[(1,4-dichloro-7-isoquinolinyl)carbonyl]amino}-3-phenylpropanoate

Chemical Property:

Purity/Quality:

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Technology Process of t-butyl DL-3-{[(1,4-dichloro-7-isoquinolinyl)carbonyl]amino}-3-phenylpropanoate

There total 5 articles about t-butyl DL-3-{[(1,4-dichloro-7-isoquinolinyl)carbonyl]amino}-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 256477-77-7
1,4-dichloro-7-isoquinolinecarbonyl chloride

: 149193-92-0
3-Amino-3-phenyl-propionic acid tert-butyl ester

: 256477-88-0
t-butyl DL-3-{[(1,4-dichloro-7-isoquinolinyl)carbonyl]amino}-3-phenylpropanoate

Guidance literature:: With hydrogenchloride; triethylamine; In dichloromethane;

Reference yield:

: 256477-74-4
ethyl 4-chloro-1-oxo-1,2-dihydro-7-isoquinolinecarboxylate

: 256477-88-0
t-butyl DL-3-{[(1,4-dichloro-7-isoquinolinyl)carbonyl]amino}-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate

2: hydrogenchloride; sodium hydroxide / tetrahydrofuran; ethanol

3: dichloromethane; N,N-dimethyl-formamide

4: hydrogenchloride; triethylamine / dichloromethane

With hydrogenchloride; sodium hydroxide; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; trichlorophosphate;

Reference yield:

: 256477-76-6
1,4-dichloro-7-isoquinolinecarboxylic acid

: 256477-88-0
t-butyl DL-3-{[(1,4-dichloro-7-isoquinolinyl)carbonyl]amino}-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane; N,N-dimethyl-formamide

2: hydrogenchloride; triethylamine / dichloromethane

With hydrogenchloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;