2'-Phenylethyl trans-2-butenesulfonate

Base Information

Chemical Name:2'-Phenylethyl trans-2-butenesulfonate
CAS No.:125452-91-7
Molecular Formula:C₁₂H₁₆O₃S
Molecular Weight:240.323
Hs Code.:

Synonyms:2'-Phenylethyl trans-2-butenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2'-Phenylethyl trans-2-butenesulfonate

Chemical Property:

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Technology Process of 2'-Phenylethyl trans-2-butenesulfonate

There total 3 articles about 2'-Phenylethyl trans-2-butenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 125452-78-0
2-Phenylethyl 1-Methylallyl Sulfite

: 125452-86-0
2'-Phenylethyl 1-methyl-2-propenesulfonate

: 125452-91-7
2'-Phenylethyl trans-2-butenesulfonate

Guidance literature:: [Pd₂(dba)₃]*benzene; triethyl phosphite; In 1,4-dioxane; for 17h; Title compound not separated from byproducts; Ambient temperature;
DOI:10.1021/jo00293a028

Reference yield: 15.0%

: 125452-77-9
2-Phenylethyl trans-2-butenyl sulfite

: 125452-86-0
2'-Phenylethyl 1-methyl-2-propenesulfonate

: 125452-91-7
2'-Phenylethyl trans-2-butenesulfonate

Guidance literature:: [Pd₂(dba)₃]*benzene; triethyl phosphite; In 1,4-dioxane; for 18h; Title compound not separated from byproducts; Ambient temperature;
DOI:10.1021/jo00293a028

Reference yield:

: 33681-75-3
2-Phenylethyl chlorosulfite

: 125452-91-7
2'-Phenylethyl trans-2-butenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / diethyl ether / 1 h / Ambient temperature

2: 15 percent / (dba)3Pd₂C₆H₆, triethyl phosphite / dioxane / 18 h / Ambient temperature

With pyridine; [Pd₂(dba)₃]*benzene; triethyl phosphite; In 1,4-dioxane; diethyl ether;
DOI:10.1021/jo00293a028