di-tert-butyl (+)-{(1S)-1-[(trityloxy)methyl]prop-2-enyl}imidodicarbonate

Base Information

Chemical Name:di-tert-butyl (+)-{(1S)-1-[(trityloxy)methyl]prop-2-enyl}imidodicarbonate
CAS No.:1099752-24-5
Molecular Formula:C₃₃H₃₉NO₅
Molecular Weight:529.676
Hs Code.:

Synonyms:di-tert-butyl (+)-{(1S)-1-[(trityloxy)methyl]prop-2-enyl}imidodicarbonate

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Chemical Property of di-tert-butyl (+)-{(1S)-1-[(trityloxy)methyl]prop-2-enyl}imidodicarbonate

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Technology Process of di-tert-butyl (+)-{(1S)-1-[(trityloxy)methyl]prop-2-enyl}imidodicarbonate

There total 2 articles about di-tert-butyl (+)-{(1S)-1-[(trityloxy)methyl]prop-2-enyl}imidodicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 949583-79-3
(E)-methyl (4-(trityloxy)but-2-en-1-yl)carbonate

: 51779-32-9
iminodicarboxylic acid di-tert-butyl ester

: 1099752-26-7
di-tert-butyl [(2E)-4-(trityloxy)but-2-en-1-yl]imidodicarbonate

: 1099752-24-5
di-tert-butyl (+)-{(1S)-1-[(trityloxy)methyl]prop-2-enyl}imidodicarbonate

Guidance literature:: (E)-methyl (4-(trityloxy)but-2-en-1-yl)carbonate; With C₅₀H₅₂IrNO₄P⁽¹⁺⁾*CF₃O₃S^(1-); 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; for 0.0833333h; Inert atmosphere; Schlenk technique;

iminodicarboxylic acid di-tert-butyl ester; In tetrahydrofuran; at 50 ℃; for 1h; enantioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1002/ejoc.201501333

Reference yield:

: 949583-79-3
(E)-methyl (4-(trityloxy)but-2-en-1-yl)carbonate

: sodium salt of di-tert-butyl iminodicarboxylate

: 1099752-26-7
di-tert-butyl [(2E)-4-(trityloxy)but-2-en-1-yl]imidodicarbonate

: 1099752-24-5
di-tert-butyl (+)-{(1S)-1-[(trityloxy)methyl]prop-2-enyl}imidodicarbonate

Guidance literature:: With bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; triethylamine; (S)-(+)-(3,5-dioxa-4-phosphacyclohepta[2,1-a;3,4-a']dinaphthalen-4-yl)-bis-[(1S)-1-(2-methoxy-phenyl)ethyl]amine; In tetrahydrofuran; at 50 ℃; for 14h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1055/s-0028-1083158