2-Pyrrolidin-1-yl-cyclohex-1-enecarboxylic acid cyclohex-1-enylamide

Base Information

Chemical Name:2-Pyrrolidin-1-yl-cyclohex-1-enecarboxylic acid cyclohex-1-enylamide
CAS No.:117919-40-1
Molecular Formula:C₁₇H₂₆N₂O
Molecular Weight:274.406
Hs Code.:

Synonyms:2-Pyrrolidin-1-yl-cyclohex-1-enecarboxylic acid cyclohex-1-enylamide

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Chemical Property of 2-Pyrrolidin-1-yl-cyclohex-1-enecarboxylic acid cyclohex-1-enylamide

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Technology Process of 2-Pyrrolidin-1-yl-cyclohex-1-enecarboxylic acid cyclohex-1-enylamide

There total 3 articles about 2-Pyrrolidin-1-yl-cyclohex-1-enecarboxylic acid cyclohex-1-enylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 636-82-8
cyclohexene-1-carboxylic acid

: 117919-40-1
2-Pyrrolidin-1-yl-cyclohex-1-enecarboxylic acid cyclohex-1-enylamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine, diphenylphosphoryl azide / toluene / 1 h, room temp., reflux, several hours

2: Ambient temperature

With diphenylphosphoranyl azide; triethylamine; In toluene;
DOI:10.1021/jo00197a061

Reference yield:

: 1125-99-1
1-(1-Cyclohexen-1-yl)pyrrolidine

: 5041-27-0
1-isocyanatocyclohex-1-ene

: 117919-40-1
2-Pyrrolidin-1-yl-cyclohex-1-enecarboxylic acid cyclohex-1-enylamide

Guidance literature:: In acetonitrile; at 20 ℃; for 8h;
DOI:10.1021/jo00262a047

Reference yield:

: 101033-15-2
1-cyclohexene-1-carbonyl azide

: 117919-40-1
2-Pyrrolidin-1-yl-cyclohex-1-enecarboxylic acid cyclohex-1-enylamide

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / Heating

2: 1.51 g / acetonitrile / 8 h / 20 °C

In acetonitrile; benzene;
DOI:10.1021/jo00262a047