N-(2-(2-nitrophenylsulfonyl)hydrazinecarbonothioyl)-5-methyl-isoxazole-4-carboxamide

Base Information

Chemical Name:N-(2-(2-nitrophenylsulfonyl)hydrazinecarbonothioyl)-5-methyl-isoxazole-4-carboxamide
CAS No.:1246456-52-9
Molecular Formula:C₁₂H₁₁N₅O₆S₂
Molecular Weight:385.381
Hs Code.:

Synonyms:N-(2-(2-nitrophenylsulfonyl)hydrazinecarbonothioyl)-5-methyl-isoxazole-4-carboxamide

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Chemical Property of N-(2-(2-nitrophenylsulfonyl)hydrazinecarbonothioyl)-5-methyl-isoxazole-4-carboxamide

Chemical Property:

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Technology Process of N-(2-(2-nitrophenylsulfonyl)hydrazinecarbonothioyl)-5-methyl-isoxazole-4-carboxamide

There total 5 articles about N-(2-(2-nitrophenylsulfonyl)hydrazinecarbonothioyl)-5-methyl-isoxazole-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆H₄N₂O₂S

: 5906-99-0
2-nitrobenzenesulfonyl hydrazide

: 1246456-52-9
N-(2-(2-nitrophenylsulfonyl)hydrazinecarbonothioyl)-5-methyl-isoxazole-4-carboxamide

Guidance literature:: In dichloromethane; at 20 ℃; for 5.5h;

Reference yield:

: 67305-24-2
5-methylisoxazole-4-carbonyl chloride

: 1246456-52-9
N-(2-(2-nitrophenylsulfonyl)hydrazinecarbonothioyl)-5-methyl-isoxazole-4-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: PEG-600 / dichloromethane / 1.5 h / 20 °C

2: dichloromethane / 5.5 h / 20 °C

With PEG-600; In dichloromethane;

Reference yield:

: 51135-73-0
5-methylisoxazole-4-carboxylic acid ethyl ester

: 1246456-52-9
N-(2-(2-nitrophenylsulfonyl)hydrazinecarbonothioyl)-5-methyl-isoxazole-4-carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride

2: thionyl chloride / Reflux

3: PEG-600 / dichloromethane / 1.5 h / 20 °C

4: dichloromethane / 5.5 h / 20 °C

With hydrogenchloride; thionyl chloride; In dichloromethane;