4-[2-(3,4-dimethylphenyl)ethyl]-1-ethyl-3-methyl-1,4,5,6,7,8-hexahydro-1,2,5-triazaazulene

Base Information

• Chemical Name: 4-[2-(3,4-dimethylphenyl)ethyl]-1-ethyl-3-methyl-1,4,5,6,7,8-hexahydro-1,2,5-triazaazulene
• CAS No.: 1010390-02-9
• Molecular Formula: C₂₀H₂₉N₃
• Molecular Weight: 311.47

Synonyms:4-[2-(3,4-dimethylphenyl)ethyl]-1-ethyl-3-methyl-1,4,5,6,7,8-hexahydro-1,2,5-triazaazulene

Chemical Property of 4-[2-(3,4-dimethylphenyl)ethyl]-1-ethyl-3-methyl-1,4,5,6,7,8-hexahydro-1,2,5-triazaazulene

Chemical Property:

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Technology Process of 4-[2-(3,4-dimethylphenyl)ethyl]-1-ethyl-3-methyl-1,4,5,6,7,8-hexahydro-1,2,5-triazaazulene

There total 1 articles about 4-[2-(3,4-dimethylphenyl)ethyl]-1-ethyl-3-methyl-1,4,5,6,7,8-hexahydro-1,2,5-triazaazulene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C20H27N3 (1010390-06-3) → 4-[2-(3,4-dimethylphenyl)ethyl]-1-ethyl-3-methyl-1,4,5,6,7,8-hexahydro-1,2,5-triazaazulene (1010390-02-9)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 0 ℃; for 1.25h;

Reference yield:

(S)-2-(methylamino)-2-oxo-1-phenylethyl 4-methylbenzenesulfonate (871224-68-9) + 4-[2-(3,4-dimethylphenyl)ethyl]-1-ethyl-3-methyl-1,4,5,6,7,8-hexahydro-1,2,5-triazaazulene (1010390-02-9) → (R)-2'-{(S)-4-[2-(3,4-dimethylphenyl)-ethyl]-1-ethyl-3-methyl-4,6,7,8-tetrahydro-1H-1,2,5-triazaazulen-5-yl}-N-methyl-2'-phenylacetamide + (R)-2'-{(R)-4-[2-(3,4-dimethylphenyl)-ethyl]-1-ethyl-3-methyl-4,6,7,8-tetrahydro-1H-1,2,5-triazaazulen-5-yl}-N-methyl-2'-phenylacetamide (1010389-84-0)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In butanone; at 70 ℃; for 23h;

upstream raw materials:

C₂₀H₂₇N₃

Downstream raw materials:

(R)-2'-{(R)-4-[2-(3,4-dimethylphenyl)-ethyl]-1-ethyl-3-methyl-4,6,7,8-tetrahydro-1H-1,2,5-triazaazulen-5-yl}-N-methyl-2'-phenylacetamide

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