Technology Process of C18H24N2O2
There total 5 articles about C18H24N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine; trichlorophosphate;
In
dichloromethane;
at 0 ℃;
Inert atmosphere;
DOI:10.1021/ja403391m
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: ethylmagnesium bromide / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere; Reflux
2.1: bis(dibenzylideneacetone)-palladium(0); tri-tert-butyl phosphine; potassium fluoride / tetrahydrofuran / 20 °C / Reflux; Inert atmosphere
3.1: sodium tetrahydroborate; cobalt(II) chloride hexahydrate / ethanol; toluene / 50 °C / Inert atmosphere
4.1: dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
5.1: trichlorophosphate; triethylamine / dichloromethane / 0 °C / Inert atmosphere
With
potassium fluoride; sodium tetrahydroborate; cobalt(II) chloride hexahydrate; tri-tert-butyl phosphine; ethylmagnesium bromide; triethylamine; bis(dibenzylideneacetone)-palladium(0); trichlorophosphate;
In
tetrahydrofuran; ethanol; dichloromethane; toluene;
DOI:10.1021/ja403391m
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere
2: trichlorophosphate; triethylamine / dichloromethane / 0 °C / Inert atmosphere
With
triethylamine; trichlorophosphate;
In
dichloromethane;
DOI:10.1021/ja403391m
