2,6-bis[3,4,5-tri(3,7-(S)-dimethyl-octyloxy)-benzoylamino]-4-iodo-toluene

Base Information

Chemical Name:2,6-bis[3,4,5-tri(3,7-(S)-dimethyl-octyloxy)-benzoylamino]-4-iodo-toluene
CAS No.:798567-80-3
Molecular Formula:C₈₁H₁₃₇IN₂O₈
Molecular Weight:1393.89
Hs Code.:

Synonyms:2,6-bis[3,4,5-tri(3,7-(S)-dimethyl-octyloxy)-benzoylamino]-4-iodo-toluene

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Chemical Property of 2,6-bis[3,4,5-tri(3,7-(S)-dimethyl-octyloxy)-benzoylamino]-4-iodo-toluene

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Technology Process of 2,6-bis[3,4,5-tri(3,7-(S)-dimethyl-octyloxy)-benzoylamino]-4-iodo-toluene

There total 7 articles about 2,6-bis[3,4,5-tri(3,7-(S)-dimethyl-octyloxy)-benzoylamino]-4-iodo-toluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 622833-05-0
3,4,5-tri((S)-3,7-dimethyloctyloxy)benzoic acid chloride

: 798567-87-0
5-iodo-2-methylbenzene-1,3-diamine

: 798567-80-3
2,6-bis[3,4,5-tri(3,7-(S)-dimethyl-octyloxy)-benzoylamino]-4-iodo-toluene

Guidance literature:: With sodium carbonate; In acetone; for 20h; Heating;
DOI:10.1021/ol048503n

Reference yield:

: 99-24-1
methyl galloate

: 798567-80-3
2,6-bis[3,4,5-tri(3,7-(S)-dimethyl-octyloxy)-benzoylamino]-4-iodo-toluene

Guidance literature:: Multi-step reaction with 5 steps

1: 27 percent / Na₂CO₃ / acetonitrile / 20 h / Heating

2: 89 percent / H₂ / Pd/C / CH₂Cl₂; ethanol; H₂O / 24 h / 30002.4 Torr

3: 90 percent / KOH / ethanol; H₂O / 12 h / Heating

4: SOCl₂ / 3 h / Heating

5: 33 percent / Na₂CO₃ / acetone / 20 h / Heating

With potassium hydroxide; thionyl chloride; hydrogen; sodium carbonate; palladium on activated charcoal; In ethanol; dichloromethane; water; acetone; acetonitrile;
DOI:10.1021/ol048503n

Reference yield:

: 10340-84-8,4895-14-1,58800-75-2,143615-81-0
(S)-citronellyl bromide

: 798567-80-3
2,6-bis[3,4,5-tri(3,7-(S)-dimethyl-octyloxy)-benzoylamino]-4-iodo-toluene

Guidance literature:: Multi-step reaction with 5 steps

1: 27 percent / Na₂CO₃ / acetonitrile / 20 h / Heating

2: 89 percent / H₂ / Pd/C / CH₂Cl₂; ethanol; H₂O / 24 h / 30002.4 Torr

3: 90 percent / KOH / ethanol; H₂O / 12 h / Heating

4: SOCl₂ / 3 h / Heating

5: 33 percent / Na₂CO₃ / acetone / 20 h / Heating

With potassium hydroxide; thionyl chloride; hydrogen; sodium carbonate; palladium on activated charcoal; In ethanol; dichloromethane; water; acetone; acetonitrile;
DOI:10.1021/ol048503n